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Synthesis of Methyl 4-Aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)-sulfamoyl]phenylamino}but-2-enoates and Their Reactions with Ninhydrin. / Gein, V. L.; Bobrovskaya, O. V.; Russkikh, A. A.; Dmitriev, M. V.; Yankin, A. N.

In: Russian Journal of Organic Chemistry, Vol. 55, No. 5, 01.05.2019, p. 602-607.

Research output: Contribution to journalArticlepeer-review

Harvard

Gein, VL, Bobrovskaya, OV, Russkikh, AA, Dmitriev, MV & Yankin, AN 2019, 'Synthesis of Methyl 4-Aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)-sulfamoyl]phenylamino}but-2-enoates and Their Reactions with Ninhydrin', Russian Journal of Organic Chemistry, vol. 55, no. 5, pp. 602-607. https://doi.org/10.1134/S107042801905004X

APA

Gein, V. L., Bobrovskaya, O. V., Russkikh, A. A., Dmitriev, M. V., & Yankin, A. N. (2019). Synthesis of Methyl 4-Aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)-sulfamoyl]phenylamino}but-2-enoates and Their Reactions with Ninhydrin. Russian Journal of Organic Chemistry, 55(5), 602-607. https://doi.org/10.1134/S107042801905004X

Vancouver

Author

Gein, V. L. ; Bobrovskaya, O. V. ; Russkikh, A. A. ; Dmitriev, M. V. ; Yankin, A. N. / Synthesis of Methyl 4-Aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)-sulfamoyl]phenylamino}but-2-enoates and Their Reactions with Ninhydrin. In: Russian Journal of Organic Chemistry. 2019 ; Vol. 55, No. 5. pp. 602-607.

BibTeX

@article{fd7a2764256d41bfa47b77a57191d830,
title = "Synthesis of Methyl 4-Aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)-sulfamoyl]phenylamino}but-2-enoates and Their Reactions with Ninhydrin",
abstract = "The reaction of methyl aroylpyruvates with 2-(4-aminobenzenesulfonamido)thiazole (norsulfazole) in acetic acid-ethanol (1: 1) afforded methyl (2Z)-4-aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)sulfamoyl]phenyl-amino} but-2-enoates which reacted with ninhydrin in glacial acetic acid to give 4-aroyl-3-{4-[(1,3-thiazol-2-yl)-sulfamoyl]phenylamino} spiro[2,5-dihydrofuran-5,2′-indane]-2,1′,3′-triones.",
keywords = "2-(4-aminobenzenesulfonamido)thiazole (norsulfazole), 4-aroyl-3-{4-[(1,3-thiazol-2-yl)sulfamoyl]-phe-nylamino} spiro[2,5-dihydrofuran-5,2′-indane]-2,1′,3′-triones, synthesis, methyl (2Z)-4-aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)sulfamoyl]phenylamino} but-2-enoates, ninhydrin, 3-thiazol-2-yl)sulfamoyl]-phe-nylamino} spiro[2, synthesis, 2 '-indane]-2, ACIDS, methyl (2Z)-4-aryl-4-oxo-2-{4-[(1, 5-dihydrofuran-5, OXALYL DERIVATIVES, KETONES, 3 '-triones, REACTION-KINETICS, ESTERS, 1 ', CHEMISTRY, 3-thiazol-2-yl)sulfamoyl]phenylamino} but-2-enoates, 4-aroyl-3-{4-[(1",
author = "Gein, {V. L.} and Bobrovskaya, {O. V.} and Russkikh, {A. A.} and Dmitriev, {M. V.} and Yankin, {A. N.}",
year = "2019",
month = may,
day = "1",
doi = "10.1134/S107042801905004X",
language = "English",
volume = "55",
pages = "602--607",
journal = "Russian Journal of Organic Chemistry",
issn = "1070-4280",
publisher = "МАИК {"}Наука/Интерпериодика{"}",
number = "5",

}

RIS

TY - JOUR

T1 - Synthesis of Methyl 4-Aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)-sulfamoyl]phenylamino}but-2-enoates and Their Reactions with Ninhydrin

AU - Gein, V. L.

AU - Bobrovskaya, O. V.

AU - Russkikh, A. A.

AU - Dmitriev, M. V.

AU - Yankin, A. N.

PY - 2019/5/1

Y1 - 2019/5/1

N2 - The reaction of methyl aroylpyruvates with 2-(4-aminobenzenesulfonamido)thiazole (norsulfazole) in acetic acid-ethanol (1: 1) afforded methyl (2Z)-4-aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)sulfamoyl]phenyl-amino} but-2-enoates which reacted with ninhydrin in glacial acetic acid to give 4-aroyl-3-{4-[(1,3-thiazol-2-yl)-sulfamoyl]phenylamino} spiro[2,5-dihydrofuran-5,2′-indane]-2,1′,3′-triones.

AB - The reaction of methyl aroylpyruvates with 2-(4-aminobenzenesulfonamido)thiazole (norsulfazole) in acetic acid-ethanol (1: 1) afforded methyl (2Z)-4-aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)sulfamoyl]phenyl-amino} but-2-enoates which reacted with ninhydrin in glacial acetic acid to give 4-aroyl-3-{4-[(1,3-thiazol-2-yl)-sulfamoyl]phenylamino} spiro[2,5-dihydrofuran-5,2′-indane]-2,1′,3′-triones.

KW - 2-(4-aminobenzenesulfonamido)thiazole (norsulfazole)

KW - 4-aroyl-3-{4-[(1,3-thiazol-2-yl)sulfamoyl]-phe-nylamino} spiro[2,5-dihydrofuran-5,2′-indane]-2,1′,3′-triones, synthesis

KW - methyl (2Z)-4-aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)sulfamoyl]phenylamino} but-2-enoates

KW - ninhydrin

KW - 3-thiazol-2-yl)sulfamoyl]-phe-nylamino} spiro[2

KW - synthesis

KW - 2 '-indane]-2

KW - ACIDS

KW - methyl (2Z)-4-aryl-4-oxo-2-{4-[(1

KW - 5-dihydrofuran-5

KW - OXALYL DERIVATIVES

KW - KETONES

KW - 3 '-triones

KW - REACTION-KINETICS

KW - ESTERS

KW - 1 '

KW - CHEMISTRY

KW - 3-thiazol-2-yl)sulfamoyl]phenylamino} but-2-enoates

KW - 4-aroyl-3-{4-[(1

UR - http://www.scopus.com/inward/record.url?scp=85068995282&partnerID=8YFLogxK

UR - http://www.mendeley.com/research/synthesis-methyl-4aryl4oxo2413thiazol2ylsulfamoylphenylaminobut2enoates-reactions-ninhydrin

U2 - 10.1134/S107042801905004X

DO - 10.1134/S107042801905004X

M3 - Article

AN - SCOPUS:85068995282

VL - 55

SP - 602

EP - 607

JO - Russian Journal of Organic Chemistry

JF - Russian Journal of Organic Chemistry

SN - 1070-4280

IS - 5

ER -

ID: 45307136