Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование
Synthesis of Methyl 4-Aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)-sulfamoyl]phenylamino}but-2-enoates and Their Reactions with Ninhydrin. / Gein, V. L.; Bobrovskaya, O. V.; Russkikh, A. A.; Dmitriev, M. V.; Yankin, A. N.
в: Russian Journal of Organic Chemistry, Том 55, № 5, 01.05.2019, стр. 602-607.Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование
}
TY - JOUR
T1 - Synthesis of Methyl 4-Aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)-sulfamoyl]phenylamino}but-2-enoates and Their Reactions with Ninhydrin
AU - Gein, V. L.
AU - Bobrovskaya, O. V.
AU - Russkikh, A. A.
AU - Dmitriev, M. V.
AU - Yankin, A. N.
PY - 2019/5/1
Y1 - 2019/5/1
N2 - The reaction of methyl aroylpyruvates with 2-(4-aminobenzenesulfonamido)thiazole (norsulfazole) in acetic acid-ethanol (1: 1) afforded methyl (2Z)-4-aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)sulfamoyl]phenyl-amino} but-2-enoates which reacted with ninhydrin in glacial acetic acid to give 4-aroyl-3-{4-[(1,3-thiazol-2-yl)-sulfamoyl]phenylamino} spiro[2,5-dihydrofuran-5,2′-indane]-2,1′,3′-triones.
AB - The reaction of methyl aroylpyruvates with 2-(4-aminobenzenesulfonamido)thiazole (norsulfazole) in acetic acid-ethanol (1: 1) afforded methyl (2Z)-4-aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)sulfamoyl]phenyl-amino} but-2-enoates which reacted with ninhydrin in glacial acetic acid to give 4-aroyl-3-{4-[(1,3-thiazol-2-yl)-sulfamoyl]phenylamino} spiro[2,5-dihydrofuran-5,2′-indane]-2,1′,3′-triones.
KW - 2-(4-aminobenzenesulfonamido)thiazole (norsulfazole)
KW - 4-aroyl-3-{4-[(1,3-thiazol-2-yl)sulfamoyl]-phe-nylamino} spiro[2,5-dihydrofuran-5,2′-indane]-2,1′,3′-triones, synthesis
KW - methyl (2Z)-4-aryl-4-oxo-2-{4-[(1,3-thiazol-2-yl)sulfamoyl]phenylamino} but-2-enoates
KW - ninhydrin
KW - 3-thiazol-2-yl)sulfamoyl]-phe-nylamino} spiro[2
KW - synthesis
KW - 2 '-indane]-2
KW - ACIDS
KW - methyl (2Z)-4-aryl-4-oxo-2-{4-[(1
KW - 5-dihydrofuran-5
KW - OXALYL DERIVATIVES
KW - KETONES
KW - 3 '-triones
KW - REACTION-KINETICS
KW - ESTERS
KW - 1 '
KW - CHEMISTRY
KW - 3-thiazol-2-yl)sulfamoyl]phenylamino} but-2-enoates
KW - 4-aroyl-3-{4-[(1
UR - http://www.scopus.com/inward/record.url?scp=85068995282&partnerID=8YFLogxK
UR - http://www.mendeley.com/research/synthesis-methyl-4aryl4oxo2413thiazol2ylsulfamoylphenylaminobut2enoates-reactions-ninhydrin
U2 - 10.1134/S107042801905004X
DO - 10.1134/S107042801905004X
M3 - Article
AN - SCOPUS:85068995282
VL - 55
SP - 602
EP - 607
JO - Russian Journal of Organic Chemistry
JF - Russian Journal of Organic Chemistry
SN - 1070-4280
IS - 5
ER -
ID: 45307136