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The study of bis-chloromethyl-phosphinic acid crystal by ATR and Raman spectroscopy and X-ray diffraction. / Glazachev, Eugeny V.; Avdontceva, Margarita S.; Asfin, Ruslan E.

In: Molecular Crystals and Liquid Crystals, Vol. 665, No. 1, 13.04.2018, p. 219-227.

Research output: Contribution to journal › Article › peer-review

Harvard

Glazachev, EV, Avdontceva, MS & Asfin, RE 2018, 'The study of bis-chloromethyl-phosphinic acid crystal by ATR and Raman spectroscopy and X-ray diffraction', Molecular Crystals and Liquid Crystals, vol. 665, no. 1, pp. 219-227. https://doi.org/10.1080/15421406.2018.1513389

APA

Glazachev, E. V., Avdontceva, M. S., & Asfin, R. E. (2018). The study of bis-chloromethyl-phosphinic acid crystal by ATR and Raman spectroscopy and X-ray diffraction. Molecular Crystals and Liquid Crystals, 665(1), 219-227. https://doi.org/10.1080/15421406.2018.1513389

Vancouver

Glazachev EV, Avdontceva MS, Asfin RE. The study of bis-chloromethyl-phosphinic acid crystal by ATR and Raman spectroscopy and X-ray diffraction. Molecular Crystals and Liquid Crystals. 2018 Apr 13;665(1):219-227. https://doi.org/10.1080/15421406.2018.1513389

Author

Glazachev, Eugeny V. ; Avdontceva, Margarita S. ; Asfin, Ruslan E. / The study of bis-chloromethyl-phosphinic acid crystal by ATR and Raman spectroscopy and X-ray diffraction. In: Molecular Crystals and Liquid Crystals. 2018 ; Vol. 665, No. 1. pp. 219-227.

BibTeX

@article{efcb3505965a4b57866db9ed1f7718d4,
title = "The study of bis-chloromethyl-phosphinic acid crystal by ATR and Raman spectroscopy and X-ray diffraction",
abstract = " Crystals of bis-chloromethyl-phosphinic acid ((CH 2 Cl) 2 POOH) are studied by attenuated total reflection (ATR) and Raman spectroscopy supported by X-Ray diffraction. The bands recorded in the ATR and in Raman spectra have the same wavenumbers within experimental uncertainty. It is in agreement with the X-Ray diffraction results which show that the molecules in crystals form infinite chains through hydrogen bonds and there is no center of inversion. The parameters of the unit cell, the bond lengths and angles, and the distance between two oxygen atoms in hydrogen bond bridges are determined. The spectral features and the intermolecular distance between oxygen atoms are characteristic for a strong hydrogen bonded system. ",
keywords = "(CH Cl) POOH, ATR spectra, crystal structure, H-bond, Raman spectra, X-Ray diffraction",
author = "Glazachev, {Eugeny V.} and Avdontceva, {Margarita S.} and Asfin, {Ruslan E.}",
year = "2018",
month = apr,
day = "13",
doi = "10.1080/15421406.2018.1513389",
language = "English",
volume = "665",
pages = "219--227",
journal = "Molecular Crystals and Liquid Crystals",
issn = "1542-1406",
publisher = "Taylor & Francis",
number = "1",

}

RIS

TY - JOUR

T1 - The study of bis-chloromethyl-phosphinic acid crystal by ATR and Raman spectroscopy and X-ray diffraction

AU - Glazachev, Eugeny V.

AU - Avdontceva, Margarita S.

AU - Asfin, Ruslan E.

PY - 2018/4/13

Y1 - 2018/4/13

N2 - Crystals of bis-chloromethyl-phosphinic acid ((CH 2 Cl) 2 POOH) are studied by attenuated total reflection (ATR) and Raman spectroscopy supported by X-Ray diffraction. The bands recorded in the ATR and in Raman spectra have the same wavenumbers within experimental uncertainty. It is in agreement with the X-Ray diffraction results which show that the molecules in crystals form infinite chains through hydrogen bonds and there is no center of inversion. The parameters of the unit cell, the bond lengths and angles, and the distance between two oxygen atoms in hydrogen bond bridges are determined. The spectral features and the intermolecular distance between oxygen atoms are characteristic for a strong hydrogen bonded system.

AB - Crystals of bis-chloromethyl-phosphinic acid ((CH 2 Cl) 2 POOH) are studied by attenuated total reflection (ATR) and Raman spectroscopy supported by X-Ray diffraction. The bands recorded in the ATR and in Raman spectra have the same wavenumbers within experimental uncertainty. It is in agreement with the X-Ray diffraction results which show that the molecules in crystals form infinite chains through hydrogen bonds and there is no center of inversion. The parameters of the unit cell, the bond lengths and angles, and the distance between two oxygen atoms in hydrogen bond bridges are determined. The spectral features and the intermolecular distance between oxygen atoms are characteristic for a strong hydrogen bonded system.

KW - (CH Cl) POOH

KW - ATR spectra

KW - crystal structure

KW - H-bond

KW - Raman spectra

KW - X-Ray diffraction

UR - http://www.scopus.com/inward/record.url?scp=85061664935&partnerID=8YFLogxK

U2 - 10.1080/15421406.2018.1513389

DO - 10.1080/15421406.2018.1513389

M3 - Article

AN - SCOPUS:85061664935

VL - 665

SP - 219

EP - 227

JO - Molecular Crystals and Liquid Crystals

JF - Molecular Crystals and Liquid Crystals

SN - 1542-1406

IS - 1

ER -

ID: 39089513