Research output: Contribution to journal › Article › peer-review
Synthesis and characterization of nanocrystalline CuCr2Se4 particles. / Kim, D.; Gedanken, A.; Tver'yanovich, Y. S.; Lee, D. W.; Kim, B. K.
In: Materials Letters, Vol. 60, No. 23, 01.10.2006, p. 2807-2809.Research output: Contribution to journal › Article › peer-review
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TY - JOUR
T1 - Synthesis and characterization of nanocrystalline CuCr2Se4 particles
AU - Kim, D.
AU - Gedanken, A.
AU - Tver'yanovich, Y. S.
AU - Lee, D. W.
AU - Kim, B. K.
PY - 2006/10/1
Y1 - 2006/10/1
N2 - A rapid and convenient polyol method with microwave irradiation was proposed to synthesize ternary chalcogenide nano-crystal, CuCr2Se4, in this study. Nano-crystalline CuCr2Se4 was formed from the chemical reaction in the mixture of cuprous chloride, chromium acetate, metallic selenium and poly ethylene glycol under microwave irradiation in argon atmosphere. Crystalline phases were identified with X-ray diffraction analysis and crystal size and morphology were examined by transmission electron microscopy. The result from thermal magnetometric analysis indicated that Curie temperature of nano-sized CuCr2Se4 was 445 K with a single phase.
AB - A rapid and convenient polyol method with microwave irradiation was proposed to synthesize ternary chalcogenide nano-crystal, CuCr2Se4, in this study. Nano-crystalline CuCr2Se4 was formed from the chemical reaction in the mixture of cuprous chloride, chromium acetate, metallic selenium and poly ethylene glycol under microwave irradiation in argon atmosphere. Crystalline phases were identified with X-ray diffraction analysis and crystal size and morphology were examined by transmission electron microscopy. The result from thermal magnetometric analysis indicated that Curie temperature of nano-sized CuCr2Se4 was 445 K with a single phase.
KW - Chalcogenide nanocrystal
KW - Magnetic semiconductor
KW - Microwave
KW - Polyol reaction
UR - http://www.scopus.com/inward/record.url?scp=33746362887&partnerID=8YFLogxK
U2 - 10.1016/j.matlet.2006.01.094
DO - 10.1016/j.matlet.2006.01.094
M3 - Article
AN - SCOPUS:33746362887
VL - 60
SP - 2807
EP - 2809
JO - Materials Letters
JF - Materials Letters
SN - 0167-577X
IS - 23
ER -
ID: 61799735