TY - JOUR

T1 - Static Headspace Analysis and Its Current Status

AU - Rodinkov, O. V.

AU - Bugaichenko, A. S.

AU - Moskvin, L. N.

PY - 2020/1/1

Y1 - 2020/1/1

N2 - Abstract: The review is devoted to the analysis of the state-of-art of the static version of headspace analysis (HSA), one of the most popular methods of sample preparation for determining, first of all, volatile organic substances in liquid and solid samples. The theoretical foundations of the method, its main regularities, and fields of application are considered. The main trends in the development of static HSA are noted: the expansion of the range of test samples and analytes and the emergence and development of combined sample preparation options based on the combination of HSA and adsorption preconcentration of analytes from the extractant gas. Technical means of HSA automation, that is, various options for liquid and solid-phase microextraction, are actively developing.

AB - Abstract: The review is devoted to the analysis of the state-of-art of the static version of headspace analysis (HSA), one of the most popular methods of sample preparation for determining, first of all, volatile organic substances in liquid and solid samples. The theoretical foundations of the method, its main regularities, and fields of application are considered. The main trends in the development of static HSA are noted: the expansion of the range of test samples and analytes and the emergence and development of combined sample preparation options based on the combination of HSA and adsorption preconcentration of analytes from the extractant gas. Technical means of HSA automation, that is, various options for liquid and solid-phase microextraction, are actively developing.

KW - gas chromatography

KW - headspace analysis

KW - sample preparation

KW - state-of-art

KW - static

KW - THIN-FILM MICROEXTRACTION

KW - GAS-CHROMATOGRAPHIC DETERMINATION

KW - RESIDUAL SOLVENTS

KW - POLYCYCLIC AROMATIC-HYDROCARBONS

KW - SOLID-PHASE MICROEXTRACTION

KW - TANDEM MASS-SPECTROMETRY

KW - SINGLE-DROP MICROEXTRACTION

KW - ESSENTIAL OIL COMPONENTS

KW - SITU DERIVATIZATION REACTION

KW - VOLATILE ORGANIC-COMPOUNDS

UR - http://www.scopus.com/inward/record.url?scp=85080075825&partnerID=8YFLogxK

UR - https://www.mendeley.com/catalogue/00053f22-e836-3c78-920b-b734414f1854/

U2 - 10.1134/S106193482001013X

DO - 10.1134/S106193482001013X

M3 - Review article

AN - SCOPUS:85080075825

VL - 75

JO - Journal of Analytical Chemistry

JF - Journal of Analytical Chemistry

SN - 1061-9348

IS - 1

ER -