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One-​Pot Synthesis and Asymmetric Oxidation of 2-​Nitro-​4-​(Trifluoromethyl)​Benzene Containing Sulfides. / Rodygin, Konstantin S.; Rubtsova, Svetlana A.; Kutchin, Alexander V.; Slepukhin, Pavel A.

In: Phosphorus, Sulfur and Silicon and the Related Elements, Vol. 186, No. 9, 2011, p. 1885-1894.

Research output: Contribution to journal › Article

Harvard

Rodygin, KS, Rubtsova, SA, Kutchin, AV & Slepukhin, PA 2011, 'One-​Pot Synthesis and Asymmetric Oxidation of 2-​Nitro-​4-​(Trifluoromethyl)​Benzene Containing Sulfides', Phosphorus, Sulfur and Silicon and the Related Elements, vol. 186, no. 9, pp. 1885-1894. https://doi.org/10.1080/10426507.2010.547893

APA

Rodygin, K. S., Rubtsova, S. A., Kutchin, A. V., & Slepukhin, P. A. (2011). One-​Pot Synthesis and Asymmetric Oxidation of 2-​Nitro-​4-​(Trifluoromethyl)​Benzene Containing Sulfides. Phosphorus, Sulfur and Silicon and the Related Elements, 186(9), 1885-1894. https://doi.org/10.1080/10426507.2010.547893

Vancouver

Rodygin KS, Rubtsova SA, Kutchin AV, Slepukhin PA. One-​Pot Synthesis and Asymmetric Oxidation of 2-​Nitro-​4-​(Trifluoromethyl)​Benzene Containing Sulfides. Phosphorus, Sulfur and Silicon and the Related Elements. 2011;186(9):1885-1894. https://doi.org/10.1080/10426507.2010.547893

Author

Rodygin, Konstantin S. ; Rubtsova, Svetlana A. ; Kutchin, Alexander V. ; Slepukhin, Pavel A. / One-​Pot Synthesis and Asymmetric Oxidation of 2-​Nitro-​4-​(Trifluoromethyl)​Benzene Containing Sulfides. In: Phosphorus, Sulfur and Silicon and the Related Elements. 2011 ; Vol. 186, No. 9. pp. 1885-1894.

BibTeX

@article{d7979d1e36984510bd53005d05797876,
title = "One-​Pot Synthesis and Asymmetric Oxidation of 2-​Nitro-​4-​(Trifluoromethyl)​Benzene Containing Sulfides",
abstract = "An efficient one-​pot method for the prepn. of 2-​nitro-​4-​(trifluoromethyl)​phenyl sulfides from 1,​1'-​disulfanediylbis[2-​nitro-​4-​(trifluoromethyl)​benzene] is proposed. The corresponding enantiomerically enriched sulfoxides with up to 78​% enantiomeric excess are prepd. by the asym. oxidn. of sulfides using a modified Sharpless method. The yield of sulfoxides decreases with an increase in the bulk of the aliph. group and with a decrease of the inductive effect of the hydrocarbon moiety on the sulfur atom.",
author = "Rodygin, {Konstantin S.} and Rubtsova, {Svetlana A.} and Kutchin, {Alexander V.} and Slepukhin, {Pavel A.}",
year = "2011",
doi = "10.1080/10426507.2010.547893",
language = "не определен",
volume = "186",
pages = "1885--1894",
journal = "Phosphorus, Sulfur and Silicon and the Related Elements",
issn = "1042-6507",
publisher = "Taylor & Francis",
number = "9",

}

RIS

TY - JOUR

T1 - One-​Pot Synthesis and Asymmetric Oxidation of 2-​Nitro-​4-​(Trifluoromethyl)​Benzene Containing Sulfides

AU - Rodygin, Konstantin S.

AU - Rubtsova, Svetlana A.

AU - Kutchin, Alexander V.

AU - Slepukhin, Pavel A.

PY - 2011

Y1 - 2011

N2 - An efficient one-​pot method for the prepn. of 2-​nitro-​4-​(trifluoromethyl)​phenyl sulfides from 1,​1'-​disulfanediylbis[2-​nitro-​4-​(trifluoromethyl)​benzene] is proposed. The corresponding enantiomerically enriched sulfoxides with up to 78​% enantiomeric excess are prepd. by the asym. oxidn. of sulfides using a modified Sharpless method. The yield of sulfoxides decreases with an increase in the bulk of the aliph. group and with a decrease of the inductive effect of the hydrocarbon moiety on the sulfur atom.

AB - An efficient one-​pot method for the prepn. of 2-​nitro-​4-​(trifluoromethyl)​phenyl sulfides from 1,​1'-​disulfanediylbis[2-​nitro-​4-​(trifluoromethyl)​benzene] is proposed. The corresponding enantiomerically enriched sulfoxides with up to 78​% enantiomeric excess are prepd. by the asym. oxidn. of sulfides using a modified Sharpless method. The yield of sulfoxides decreases with an increase in the bulk of the aliph. group and with a decrease of the inductive effect of the hydrocarbon moiety on the sulfur atom.

U2 - 10.1080/10426507.2010.547893

DO - 10.1080/10426507.2010.547893

M3 - статья

VL - 186

SP - 1885

EP - 1894

JO - Phosphorus, Sulfur and Silicon and the Related Elements

JF - Phosphorus, Sulfur and Silicon and the Related Elements

SN - 1042-6507

IS - 9

ER -

ID: 5551397