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2+1 Rhenium Tricarbonyl Complexes with N,N′-Bidentate Ligands and Ethyl Isocyanoacetate : Synthesis, Structure, and Properties. / Tyupina, M. Yu; Miroslavov, A. E.; Sidorenko, G. V.; Gurzhiy, V. V.; Sakhonenkova, A. P.

In: Russian Journal of General Chemistry, Vol. 92, No. 1, 01.2022, p. 69-78.

Research output: Contribution to journal › Article › peer-review

Harvard

Tyupina, MY, Miroslavov, AE, Sidorenko, GV, Gurzhiy, VV & Sakhonenkova, AP 2022, '2+1 Rhenium Tricarbonyl Complexes with N,N′-Bidentate Ligands and Ethyl Isocyanoacetate: Synthesis, Structure, and Properties', Russian Journal of General Chemistry, vol. 92, no. 1, pp. 69-78. https://doi.org/10.1134/s1070363222010108

APA

Tyupina, M. Y., Miroslavov, A. E., Sidorenko, G. V., Gurzhiy, V. V., & Sakhonenkova, A. P. (2022). 2+1 Rhenium Tricarbonyl Complexes with N,N′-Bidentate Ligands and Ethyl Isocyanoacetate: Synthesis, Structure, and Properties. Russian Journal of General Chemistry, 92(1), 69-78. https://doi.org/10.1134/s1070363222010108

Vancouver

Tyupina MY, Miroslavov AE, Sidorenko GV, Gurzhiy VV, Sakhonenkova AP. 2+1 Rhenium Tricarbonyl Complexes with N,N′-Bidentate Ligands and Ethyl Isocyanoacetate: Synthesis, Structure, and Properties. Russian Journal of General Chemistry. 2022 Jan;92(1):69-78. https://doi.org/10.1134/s1070363222010108

Author

Tyupina, M. Yu ; Miroslavov, A. E. ; Sidorenko, G. V. ; Gurzhiy, V. V. ; Sakhonenkova, A. P. / 2+1 Rhenium Tricarbonyl Complexes with N,N′-Bidentate Ligands and Ethyl Isocyanoacetate : Synthesis, Structure, and Properties. In: Russian Journal of General Chemistry. 2022 ; Vol. 92, No. 1. pp. 69-78.

BibTeX

@article{6c9462b43f6e43cbbd2f3d32ec728629,
title = "2+1 Rhenium Tricarbonyl Complexes with N,N′-Bidentate Ligands and Ethyl Isocyanoacetate: Synthesis, Structure, and Properties",
abstract = "Abstract: 2+1 tricarbonyl complexes [Re(CO)3(N^N)CNCH2COOEt]X, where N^N = 2,2′-bipyridine (bipy) or 1,10-phenanthroline (phen) and X = Cl– or ClO4–, were prepared and isolated by two procedures. The intermediate tricarbonyl complexes [Re(CO)3(N^N)X] (where X = Cl– or ClO4–) were also isolated. The composition and molecular structure of these complexes were determined by single crystal X-ray diffraction analysis. The complexes have fac-tricarbonyl structure with bidentate coordination of bipy and phen. The complexes were characterized by PL, IR, UV-Vis, and 1H NMR spectroscopy and by elemental analysis.",
keywords = "bipyridine, ethyl isocyanoacetate, phenanthroline, rhenium, single crystal X-ray diffraction, spectroscopy, tricarbonyl complexes",
author = "Tyupina, {M. Yu} and Miroslavov, {A. E.} and Sidorenko, {G. V.} and Gurzhiy, {V. V.} and Sakhonenkova, {A. P.}",
note = "Tyupina, M.Y., Miroslavov, A.E., Sidorenko, G.V. et al. 2+1 Rhenium Tricarbonyl Complexes with N,N′-Bidentate Ligands and Ethyl Isocyanoacetate: Synthesis, Structure, and Properties. Russ J Gen Chem 92, 69–78 (2022). https://doi.org/10.1134/S1070363222010108",
year = "2022",
month = jan,
doi = "10.1134/s1070363222010108",
language = "English",
volume = "92",
pages = "69--78",
journal = "Russian Journal of General Chemistry",
issn = "1070-3632",
publisher = "МАИК {"}Наука/Интерпериодика{"}",
number = "1",

}

RIS

TY - JOUR

T1 - 2+1 Rhenium Tricarbonyl Complexes with N,N′-Bidentate Ligands and Ethyl Isocyanoacetate

T2 - Synthesis, Structure, and Properties

AU - Tyupina, M. Yu

AU - Miroslavov, A. E.

AU - Sidorenko, G. V.

AU - Gurzhiy, V. V.

AU - Sakhonenkova, A. P.

N1 - Tyupina, M.Y., Miroslavov, A.E., Sidorenko, G.V. et al. 2+1 Rhenium Tricarbonyl Complexes with N,N′-Bidentate Ligands and Ethyl Isocyanoacetate: Synthesis, Structure, and Properties. Russ J Gen Chem 92, 69–78 (2022). https://doi.org/10.1134/S1070363222010108

PY - 2022/1

Y1 - 2022/1

N2 - Abstract: 2+1 tricarbonyl complexes [Re(CO)3(N^N)CNCH2COOEt]X, where N^N = 2,2′-bipyridine (bipy) or 1,10-phenanthroline (phen) and X = Cl– or ClO4–, were prepared and isolated by two procedures. The intermediate tricarbonyl complexes [Re(CO)3(N^N)X] (where X = Cl– or ClO4–) were also isolated. The composition and molecular structure of these complexes were determined by single crystal X-ray diffraction analysis. The complexes have fac-tricarbonyl structure with bidentate coordination of bipy and phen. The complexes were characterized by PL, IR, UV-Vis, and 1H NMR spectroscopy and by elemental analysis.

AB - Abstract: 2+1 tricarbonyl complexes [Re(CO)3(N^N)CNCH2COOEt]X, where N^N = 2,2′-bipyridine (bipy) or 1,10-phenanthroline (phen) and X = Cl– or ClO4–, were prepared and isolated by two procedures. The intermediate tricarbonyl complexes [Re(CO)3(N^N)X] (where X = Cl– or ClO4–) were also isolated. The composition and molecular structure of these complexes were determined by single crystal X-ray diffraction analysis. The complexes have fac-tricarbonyl structure with bidentate coordination of bipy and phen. The complexes were characterized by PL, IR, UV-Vis, and 1H NMR spectroscopy and by elemental analysis.

KW - bipyridine

KW - ethyl isocyanoacetate

KW - phenanthroline

KW - rhenium

KW - single crystal X-ray diffraction

KW - spectroscopy

KW - tricarbonyl complexes

UR - http://www.scopus.com/inward/record.url?scp=85125091277&partnerID=8YFLogxK

UR - https://www.mendeley.com/catalogue/6204424f-f87e-308c-bf74-14f98b1d7814/

U2 - 10.1134/s1070363222010108

DO - 10.1134/s1070363222010108

M3 - Article

AN - SCOPUS:85125091277

VL - 92

SP - 69

EP - 78

JO - Russian Journal of General Chemistry

JF - Russian Journal of General Chemistry

SN - 1070-3632

IS - 1

ER -

ID: 98952920