• А.С. Михердов
  • С.В. Байков
  • И. К. Прокусина
  • А.А. Шетнев
  • А. Д. Котов
The reaction of bis(cyclohexylisocyanide) complex of Pd(II) with substituted benzo[ d ]thiazole-2-amines in the presence of triethanolamine as the base leads to the formation of deprotonated C , N -chelated carbene complexes with a structure similar to that described previously for the reaction products with unsubstituted benzo[ d ]thiazole-2-amine. The complexes were isolated in pure form and characterized using high resolution mass spectrometry, IR and NMR spectroscopy (1H, 13C{1H}, 1H-1H COSY, 1H-1H NOESY, 1H-13C HSQC, 1H-13C HMBC). The resulting complexes exhibit moderate antibacterial activity against sensitive strains of gram-negative bacteria E. coli (C600) and P. fluorescens (P218), gram-positive bacteria S. aureus (ATCC-25923) and B. subtillis (VKM B3142D), as well as fungi C. albicans (VKPGU-401/885-653).
Translated title of the contributionSynthesis and Properties of C,N-Chelated Carbene Complexes of Palladium(II) with 2-Aminobenzo[d]thiazole Fragment
Original languageRussian
Pages (from-to)1572-1579
Number of pages8
JournalЖУРНАЛ ОБЩЕЙ ХИМИИ
Volume89
Issue number10
DOIs
StatePublished - Sep 2019

    Scopus subject areas

  • Organic Chemistry

    Research areas

  • acyclic diaminocarbene complexes, antimicrobial activity, benzo[d]thiazole-2-amines, Isocyanide ligands, palladium chelate complexes, антимикробная активность, ациклические диаминокарбеновые комплексы, бензо[d]тиазол-2-амины, изоцианидные лиганды, хелатные комплексы палладия

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