Synthesis of N,N'-Disubstituted Dithiooxamide Derivatives by the Modified Willgerodt–Kindler Reaction

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Synthesis of N,N'-Disubstituted Dithiooxamide Derivatives by the Modified Willgerodt–Kindler Reaction. / Боярский, Вадим Павлович; Елисеенков, Евгений Владимирович; Петров, Александр Анатольевич; Пономарёва, Татьяна Николаевна.

в: Russian Journal of Organic Chemistry, Том 56, № 5, 01.05.2020, стр. 781-787.

Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование

Author

Боярский, Вадим Павлович ; Елисеенков, Евгений Владимирович ; Петров, Александр Анатольевич ; Пономарёва, Татьяна Николаевна. / Synthesis of N,N'-Disubstituted Dithiooxamide Derivatives by the Modified Willgerodt–Kindler Reaction. в: Russian Journal of Organic Chemistry. 2020 ; Том 56, № 5. стр. 781-787.

BibTeX

@article{3ab77c75f2a241879e590add7beb93e3,

title = "Synthesis of N,N'-Disubstituted Dithiooxamide Derivatives by the Modified Willgerodt–Kindler Reaction",

abstract = "The conditions of the reaction of trichloroethylene with sulfur and amines were optimized (the modified Willgerodt-Kindler reaction). The reaction of tetrachloroethylene with sulfur and some basic primary and secondary amines of the aliphatic series in DMF under mild conditions leads toN,N'-disubstituted dithiooxamides in 30-70% yields and with a 100% conversion of tetrachloroethylene.",

keywords = "N,N'-disubstituted dithiooxamide, Willgerodt–Kindler reaction, tetrachloroethylene, COMPLEXES, Willgerodt-Kindler reaction, SULFUR, THIOAMIDES, N'-disubstituted dithiooxamide, N",

author = "Боярский, {Вадим Павлович} and Елисеенков, {Евгений Владимирович} and Петров, {Александр Анатольевич} and Пономарёва, {Татьяна Николаевна}",

note = "Publisher Copyright: {\textcopyright} 2020, Pleiades Publishing, Ltd.",

year = "2020",

month = may,

day = "1",

doi = "10.1134/S1070428020050097",

language = "English",

volume = "56",

pages = "781--787",

journal = "Russian Journal of Organic Chemistry",

issn = "1070-4280",

publisher = "МАИК {"}Наука/Интерпериодика{"}",

number = "5",

}

RIS

TY - JOUR

T1 - Synthesis of N,N'-Disubstituted Dithiooxamide Derivatives by the Modified Willgerodt–Kindler Reaction

AU - Боярский, Вадим Павлович

AU - Елисеенков, Евгений Владимирович

AU - Петров, Александр Анатольевич

AU - Пономарёва, Татьяна Николаевна

PY - 2020/5/1

Y1 - 2020/5/1

N2 - The conditions of the reaction of trichloroethylene with sulfur and amines were optimized (the modified Willgerodt-Kindler reaction). The reaction of tetrachloroethylene with sulfur and some basic primary and secondary amines of the aliphatic series in DMF under mild conditions leads toN,N'-disubstituted dithiooxamides in 30-70% yields and with a 100% conversion of tetrachloroethylene.

AB - The conditions of the reaction of trichloroethylene with sulfur and amines were optimized (the modified Willgerodt-Kindler reaction). The reaction of tetrachloroethylene with sulfur and some basic primary and secondary amines of the aliphatic series in DMF under mild conditions leads toN,N'-disubstituted dithiooxamides in 30-70% yields and with a 100% conversion of tetrachloroethylene.

KW - N,N'-disubstituted dithiooxamide

KW - Willgerodt–Kindler reaction

KW - tetrachloroethylene

KW - COMPLEXES

KW - Willgerodt-Kindler reaction

KW - SULFUR

KW - THIOAMIDES

KW - N'-disubstituted dithiooxamide

KW - N

UR - http://www.scopus.com/inward/record.url?scp=85086831912&partnerID=8YFLogxK

U2 - 10.1134/S1070428020050097

DO - 10.1134/S1070428020050097

M3 - Article

VL - 56

SP - 781

EP - 787

JO - Russian Journal of Organic Chemistry

JF - Russian Journal of Organic Chemistry

SN - 1070-4280

IS - 5

ER -

ID: 60494035