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Synthesis of Mono- and Disaccharide 4-[(ω-Sulfanylalkyl)oxy]benzoylhydrazones as Potential Glycoligands for Noble Metal Nanoparticles. / Ershov, A. Yu; Martynenkov, A. A.; Lagoda, I. V.; Yakimansky, A. V.

в: Russian Journal of General Chemistry, Том 89, № 2, 01.02.2019, стр. 292-299.

Результаты исследований: Научные публикации в периодических изданияхстатьяРецензирование

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Author

Ershov, A. Yu ; Martynenkov, A. A. ; Lagoda, I. V. ; Yakimansky, A. V. / Synthesis of Mono- and Disaccharide 4-[(ω-Sulfanylalkyl)oxy]benzoylhydrazones as Potential Glycoligands for Noble Metal Nanoparticles. в: Russian Journal of General Chemistry. 2019 ; Том 89, № 2. стр. 292-299.

BibTeX

@article{92d5f7a1357c46ee963720f3929a1f74,
title = "Synthesis of Mono- and Disaccharide 4-[(ω-Sulfanylalkyl)oxy]benzoylhydrazones as Potential Glycoligands for Noble Metal Nanoparticles",
abstract = " A procedure has been developed for the synthesis of previously unknown aldose 4-[(ω-sulfanylalkyl) oxy]benzoylhydrazones (where alkyl is hexyl or decyl and aldoses are D-glucose, D-galactose, D-maltose, and D-lactose) that a repromising glycoligands for noble metal nanoparticles. According to the 1 H and 13 C NMR data, 4-[(ω-sulfanylalkyl)oxy]benzoylhydrazones derived from D-glucose, D-maltose, and D-lactose in crystal and in DMSO-d 6 solution have exclusively the cyclic pyranose structure (α- and β-anomers). D-Galactose 4-[(ω-sulfanylalkyl)oxy]benzoylhydrazones in DMSO-d 6 solution exist as tautomeric mixtures of cyclic pyranose and open-chain acylhydrazone structures. ",
keywords = "ring—chain tautomerism, thiol-containing mono- and disaccharide acylhydrazones",
author = "Ershov, {A. Yu} and Martynenkov, {A. A.} and Lagoda, {I. V.} and Yakimansky, {A. V.}",
year = "2019",
month = feb,
day = "1",
doi = "10.1134/S1070363219020208",
language = "English",
volume = "89",
pages = "292--299",
journal = "Russian Journal of General Chemistry",
issn = "1070-3632",
publisher = "МАИК {"}Наука/Интерпериодика{"}",
number = "2",

}

RIS

TY - JOUR

T1 - Synthesis of Mono- and Disaccharide 4-[(ω-Sulfanylalkyl)oxy]benzoylhydrazones as Potential Glycoligands for Noble Metal Nanoparticles

AU - Ershov, A. Yu

AU - Martynenkov, A. A.

AU - Lagoda, I. V.

AU - Yakimansky, A. V.

PY - 2019/2/1

Y1 - 2019/2/1

N2 - A procedure has been developed for the synthesis of previously unknown aldose 4-[(ω-sulfanylalkyl) oxy]benzoylhydrazones (where alkyl is hexyl or decyl and aldoses are D-glucose, D-galactose, D-maltose, and D-lactose) that a repromising glycoligands for noble metal nanoparticles. According to the 1 H and 13 C NMR data, 4-[(ω-sulfanylalkyl)oxy]benzoylhydrazones derived from D-glucose, D-maltose, and D-lactose in crystal and in DMSO-d 6 solution have exclusively the cyclic pyranose structure (α- and β-anomers). D-Galactose 4-[(ω-sulfanylalkyl)oxy]benzoylhydrazones in DMSO-d 6 solution exist as tautomeric mixtures of cyclic pyranose and open-chain acylhydrazone structures.

AB - A procedure has been developed for the synthesis of previously unknown aldose 4-[(ω-sulfanylalkyl) oxy]benzoylhydrazones (where alkyl is hexyl or decyl and aldoses are D-glucose, D-galactose, D-maltose, and D-lactose) that a repromising glycoligands for noble metal nanoparticles. According to the 1 H and 13 C NMR data, 4-[(ω-sulfanylalkyl)oxy]benzoylhydrazones derived from D-glucose, D-maltose, and D-lactose in crystal and in DMSO-d 6 solution have exclusively the cyclic pyranose structure (α- and β-anomers). D-Galactose 4-[(ω-sulfanylalkyl)oxy]benzoylhydrazones in DMSO-d 6 solution exist as tautomeric mixtures of cyclic pyranose and open-chain acylhydrazone structures.

KW - ring—chain tautomerism

KW - thiol-containing mono- and disaccharide acylhydrazones

UR - http://www.scopus.com/inward/record.url?scp=85063995174&partnerID=8YFLogxK

U2 - 10.1134/S1070363219020208

DO - 10.1134/S1070363219020208

M3 - Article

AN - SCOPUS:85063995174

VL - 89

SP - 292

EP - 299

JO - Russian Journal of General Chemistry

JF - Russian Journal of General Chemistry

SN - 1070-3632

IS - 2

ER -

ID: 50556409