Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование
Synthesis by successive ionic layer deposition on the silica surface and study of NiO1-x·zH2O nanolayers. / Tolstobrov, E. V.; Tolstoi, V. P.
в: Russian Journal of General Chemistry, Том 69, № 6, 01.12.1999, стр. 856-860.Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование
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TY - JOUR
T1 - Synthesis by successive ionic layer deposition on the silica surface and study of NiO1-x·zH2O nanolayers
AU - Tolstobrov, E. V.
AU - Tolstoi, V. P.
PY - 1999/12/1
Y1 - 1999/12/1
N2 - The possibility of preparing NiO1-x·zH2O nanolayers on the silica surface by successive ionic layer deposition was demonstrated for the first time. Effects of the concentration and pH of reagent solutions and washing liquids, of the time of treating with them, and of the number of ionic layer deposition cycles on the kinetics of nanolayer growth were studied. Conditions were found for the formation of nanolayers by reactions of sorbed ions in a layer. The composition of the resulting layers was studied by the UV-Vis and IR Fourier spectroscopy and by chemical analysis. Their thickness was determined ellipsometrically. The synthesis yields layers of nickel peroxide compounds, their thickness being determined by the number of ionic layer deposition cycles at a level of nanometer fractions. Changes in the compositions of the nanolayers on keeping and heating in air were also studied.
AB - The possibility of preparing NiO1-x·zH2O nanolayers on the silica surface by successive ionic layer deposition was demonstrated for the first time. Effects of the concentration and pH of reagent solutions and washing liquids, of the time of treating with them, and of the number of ionic layer deposition cycles on the kinetics of nanolayer growth were studied. Conditions were found for the formation of nanolayers by reactions of sorbed ions in a layer. The composition of the resulting layers was studied by the UV-Vis and IR Fourier spectroscopy and by chemical analysis. Their thickness was determined ellipsometrically. The synthesis yields layers of nickel peroxide compounds, their thickness being determined by the number of ionic layer deposition cycles at a level of nanometer fractions. Changes in the compositions of the nanolayers on keeping and heating in air were also studied.
UR - http://www.scopus.com/inward/record.url?scp=0033474250&partnerID=8YFLogxK
M3 - Article
AN - SCOPUS:0033474250
VL - 69
SP - 856
EP - 860
JO - Russian Journal of General Chemistry
JF - Russian Journal of General Chemistry
SN - 1070-3632
IS - 6
ER -
ID: 42175268