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Synthesis and crystal structure of Pb 3O 2(SeO 3). / Krivovichev, Sergey V.; Avdontseva, Evgeniya Yu; Burns, Peter C.

в: Zeitschrift fur Anorganische und Allgemeine Chemie, Том 630, № 4, 01.04.2004, стр. 558-562.

Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование

Harvard

Krivovichev, SV, Avdontseva, EY & Burns, PC 2004, 'Synthesis and crystal structure of Pb 3O 2(SeO 3)', Zeitschrift fur Anorganische und Allgemeine Chemie, Том. 630, № 4, стр. 558-562. https://doi.org/10.1002/zaac.200300291

APA

Krivovichev, S. V., Avdontseva, E. Y., & Burns, P. C. (2004). Synthesis and crystal structure of Pb 3O 2(SeO 3). Zeitschrift fur Anorganische und Allgemeine Chemie, 630(4), 558-562. https://doi.org/10.1002/zaac.200300291

Vancouver

Krivovichev SV, Avdontseva EY, Burns PC. Synthesis and crystal structure of Pb 3O 2(SeO 3). Zeitschrift fur Anorganische und Allgemeine Chemie. 2004 Апр. 1;630(4):558-562. https://doi.org/10.1002/zaac.200300291

Author

Krivovichev, Sergey V. ; Avdontseva, Evgeniya Yu ; Burns, Peter C. / Synthesis and crystal structure of Pb 3O 2(SeO 3). в: Zeitschrift fur Anorganische und Allgemeine Chemie. 2004 ; Том 630, № 4. стр. 558-562.

BibTeX

@article{a8da75f83ca04e6cbede03636da245f4,
title = "Synthesis and crystal structure of Pb 3O 2(SeO 3)",
abstract = "Single crystals of Pb 3O 2(SeO 3) have been prepared hydro thermally at 230°C. The structure (orthorhombic, Cmc2 1, a = 10.529(2), b = 10.722(2), c = 5.7527(12) {\AA}, V = 649.5(2) {\AA} 3) has been solved by direct methods and refined to R 1 = 0.059 on the basis of 615 unique observed reflections (|F o| = 4σ F). The structure is based upon double [O 2Pb 3] 2+ chains of edge-sharing [OPb 4] 6+ tetrahedra. These [O 2Pb 3] 2+ chains run parallel to [001], and their planes are parallel to (010). The pyramidal (SeO 3) 2 anions are located between the chains; their triangular oxygen atom bases lie parallel to (001) and all (SeO 3) 2- groups are pointing in the same direction. A short compilation of [O 2M 3] chains of oxocentred M 4 tetrahedra in minerals and inorganic compounds is provided.",
keywords = "Crystal structures, Lead, Lead oxide selelenite, Selenium",
author = "Krivovichev, {Sergey V.} and Avdontseva, {Evgeniya Yu} and Burns, {Peter C.}",
year = "2004",
month = apr,
day = "1",
doi = "10.1002/zaac.200300291",
language = "English",
volume = "630",
pages = "558--562",
journal = "Zeitschrift fur Anorganische und Allgemeine Chemie",
issn = "0044-2313",
publisher = "Wiley-Blackwell",
number = "4",

}

RIS

TY - JOUR

T1 - Synthesis and crystal structure of Pb 3O 2(SeO 3)

AU - Krivovichev, Sergey V.

AU - Avdontseva, Evgeniya Yu

AU - Burns, Peter C.

PY - 2004/4/1

Y1 - 2004/4/1

N2 - Single crystals of Pb 3O 2(SeO 3) have been prepared hydro thermally at 230°C. The structure (orthorhombic, Cmc2 1, a = 10.529(2), b = 10.722(2), c = 5.7527(12) Å, V = 649.5(2) Å 3) has been solved by direct methods and refined to R 1 = 0.059 on the basis of 615 unique observed reflections (|F o| = 4σ F). The structure is based upon double [O 2Pb 3] 2+ chains of edge-sharing [OPb 4] 6+ tetrahedra. These [O 2Pb 3] 2+ chains run parallel to [001], and their planes are parallel to (010). The pyramidal (SeO 3) 2 anions are located between the chains; their triangular oxygen atom bases lie parallel to (001) and all (SeO 3) 2- groups are pointing in the same direction. A short compilation of [O 2M 3] chains of oxocentred M 4 tetrahedra in minerals and inorganic compounds is provided.

AB - Single crystals of Pb 3O 2(SeO 3) have been prepared hydro thermally at 230°C. The structure (orthorhombic, Cmc2 1, a = 10.529(2), b = 10.722(2), c = 5.7527(12) Å, V = 649.5(2) Å 3) has been solved by direct methods and refined to R 1 = 0.059 on the basis of 615 unique observed reflections (|F o| = 4σ F). The structure is based upon double [O 2Pb 3] 2+ chains of edge-sharing [OPb 4] 6+ tetrahedra. These [O 2Pb 3] 2+ chains run parallel to [001], and their planes are parallel to (010). The pyramidal (SeO 3) 2 anions are located between the chains; their triangular oxygen atom bases lie parallel to (001) and all (SeO 3) 2- groups are pointing in the same direction. A short compilation of [O 2M 3] chains of oxocentred M 4 tetrahedra in minerals and inorganic compounds is provided.

KW - Crystal structures

KW - Lead

KW - Lead oxide selelenite

KW - Selenium

UR - http://www.scopus.com/inward/record.url?scp=4644294004&partnerID=8YFLogxK

U2 - 10.1002/zaac.200300291

DO - 10.1002/zaac.200300291

M3 - Article

AN - SCOPUS:4644294004

VL - 630

SP - 558

EP - 562

JO - Zeitschrift fur Anorganische und Allgemeine Chemie

JF - Zeitschrift fur Anorganische und Allgemeine Chemie

SN - 0044-2313

IS - 4

ER -

ID: 49258186