DOI

Substituted N-(pyridin-2-yl) ureas or carbamates act as polynucleophiles upon the reaction with palladium(II) bis(isocyanide) complexes at RT to give metallacycles containing azaheterocyclic and urea fragments. Nine new C,N-chelate deprotonated diaminocarbene palladium(II) complexes were synthesized by coupling substituted N-(2-pyridyl)ureas and coordinated isocyanides. The obtained yellow or green-yellow species were characterized by high-resolution mass spectrometry and 1D (1H, 13C) NMR spectroscopies. The structures of six complexes in a solid state were elucidated by single-crystal X-ray diffraction (XRD). This universal and convenient method for the preparation of C^N-cyclometallated palladium(II) complexes under mild conditions opens the way to the targeted synthesis of polyfunctional organometallic compounds that combine the chemical, biological, and photophysical properties of metallacycles and parent azaheterocycles.
Язык оригиналаанглийский
Номер статьи122518
ЖурналJournal of Organometallic Chemistry
Том980-981
Дата раннего онлайн-доступа16 сен 2022
DOI
СостояниеОпубликовано - 1 дек 2022

    Предметные области Scopus

  • Химия материалов
  • Биохимия
  • Неорганическая химия
  • Физическая и теоретическая химия
  • Органическая химия

ID: 99947819