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One-pot preparation of methyl 2-diazo-3-oxopropionates comprising an aqueous ‘sulfonyl-azide-free’ (SAFE) diazo transfer step. / Zhmurov, Petr A.; Dar'in, Dmitry V.; Bakulina, Olga Yu; Krasavin, Mikhail.

в: Mendeleev Communications , Том 30, № 3, 2020, стр. 311-312.

Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование

Harvard

Zhmurov, PA, Dar'in, DV, Bakulina, OY & Krasavin, M 2020, 'One-pot preparation of methyl 2-diazo-3-oxopropionates comprising an aqueous ‘sulfonyl-azide-free’ (SAFE) diazo transfer step', Mendeleev Communications , Том. 30, № 3, стр. 311-312. https://doi.org/10.1016/j.mencom.2020.05.016

APA

Zhmurov, P. A., Dar'in, D. V., Bakulina, O. Y., & Krasavin, M. (2020). One-pot preparation of methyl 2-diazo-3-oxopropionates comprising an aqueous ‘sulfonyl-azide-free’ (SAFE) diazo transfer step. Mendeleev Communications , 30(3), 311-312. https://doi.org/10.1016/j.mencom.2020.05.016

Vancouver

Zhmurov PA, Dar'in DV, Bakulina OY, Krasavin M. One-pot preparation of methyl 2-diazo-3-oxopropionates comprising an aqueous ‘sulfonyl-azide-free’ (SAFE) diazo transfer step. Mendeleev Communications . 2020;30(3):311-312. https://doi.org/10.1016/j.mencom.2020.05.016

Author

Zhmurov, Petr A. ; Dar'in, Dmitry V. ; Bakulina, Olga Yu ; Krasavin, Mikhail. / One-pot preparation of methyl 2-diazo-3-oxopropionates comprising an aqueous ‘sulfonyl-azide-free’ (SAFE) diazo transfer step. в: Mendeleev Communications . 2020 ; Том 30, № 3. стр. 311-312.

BibTeX

@article{53dbadf9a55048898d78379a4cdf4ac8,
title = "One-pot preparation of methyl 2-diazo-3-oxopropionates comprising an aqueous {\textquoteleft}sulfonyl-azide-free{\textquoteright} (SAFE) diazo transfer step",
abstract = "Methyl 2-diazo-3-oxopropionates were obtained by in situ methoxycarbonylation of methyl ketones followed by diazo transfer onto active methylene group of the intermediate beta-oxo esters. At the second stage, 'sulfonyl-azide-free' (SAFE) diazo transfer protocol in aqueous medium was employed.",
keywords = "diazo transfer, insertion reactions, methoxycarbonylation, SAFE cocktail, β-oxopropionates, KETONES, beta-oxopropionates, PROTOCOL",
author = "Zhmurov, {Petr A.} and Dar'in, {Dmitry V.} and Bakulina, {Olga Yu} and Mikhail Krasavin",
year = "2020",
doi = "10.1016/j.mencom.2020.05.016",
language = "English",
volume = "30",
pages = "311--312",
journal = "Mendeleev Communications",
issn = "0959-9436",
publisher = "Elsevier",
number = "3",

}

RIS

TY - JOUR

T1 - One-pot preparation of methyl 2-diazo-3-oxopropionates comprising an aqueous ‘sulfonyl-azide-free’ (SAFE) diazo transfer step

AU - Zhmurov, Petr A.

AU - Dar'in, Dmitry V.

AU - Bakulina, Olga Yu

AU - Krasavin, Mikhail

PY - 2020

Y1 - 2020

N2 - Methyl 2-diazo-3-oxopropionates were obtained by in situ methoxycarbonylation of methyl ketones followed by diazo transfer onto active methylene group of the intermediate beta-oxo esters. At the second stage, 'sulfonyl-azide-free' (SAFE) diazo transfer protocol in aqueous medium was employed.

AB - Methyl 2-diazo-3-oxopropionates were obtained by in situ methoxycarbonylation of methyl ketones followed by diazo transfer onto active methylene group of the intermediate beta-oxo esters. At the second stage, 'sulfonyl-azide-free' (SAFE) diazo transfer protocol in aqueous medium was employed.

KW - diazo transfer

KW - insertion reactions

KW - methoxycarbonylation

KW - SAFE cocktail

KW - β-oxopropionates

KW - KETONES

KW - beta-oxopropionates

KW - PROTOCOL

UR - http://www.scopus.com/inward/record.url?scp=85085979027&partnerID=8YFLogxK

UR - https://www.mendeley.com/catalogue/3629bcdd-c770-3880-a506-0b1560ba1484/

U2 - 10.1016/j.mencom.2020.05.016

DO - 10.1016/j.mencom.2020.05.016

M3 - Article

AN - SCOPUS:85085979027

VL - 30

SP - 311

EP - 312

JO - Mendeleev Communications

JF - Mendeleev Communications

SN - 0959-9436

IS - 3

ER -

ID: 59755965