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On the Nature of Defects in Mn1 –xFe xGe Compounds Synthesized under High Pressure. / Iashina, E. G.; Altynbaev, E. V.; Fomicheva, L. N.; Tsvyashchenko, A. V.; Grigoriev, S. V.
в: Journal of Surface Investigation, Том 14, № 3, 01.05.2020, стр. 429-433.Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование
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TY - JOUR
T1 - On the Nature of Defects in Mn1 –xFe xGe Compounds Synthesized under High Pressure
AU - Iashina, E. G.
AU - Altynbaev, E. V.
AU - Fomicheva, L. N.
AU - Tsvyashchenko, A. V.
AU - Grigoriev, S. V.
N1 - Publisher Copyright: © 2020, Pleiades Publishing, Ltd.
PY - 2020/5/1
Y1 - 2020/5/1
N2 - Abstract: The mesostructure of Mn1 – xFex Ge transition-metal monogermanides is studied by small-angle neutron scattering (SANS) and ultra-SANS in a wide concentration range of x = 0.0–1.0.It is shown that the main contribution to the scattering intensity for all concentrations x is made by scattering at crystallites with sharp boundaries and sizes of 1–10 μm, which is described by the squared Lorentzian function. An additional contribution to the scattering intensity as a result of scattering at an ensemble of defects is found as well, which is characteristic of manganese-rich samples. This contribution is well fitted by the power function Q–n with the exponent n = 3. The complementary scattering typical of iron-rich samples is described by an exponential function and also seems to be a part of scattering at sharp-boundary crystallites.
AB - Abstract: The mesostructure of Mn1 – xFex Ge transition-metal monogermanides is studied by small-angle neutron scattering (SANS) and ultra-SANS in a wide concentration range of x = 0.0–1.0.It is shown that the main contribution to the scattering intensity for all concentrations x is made by scattering at crystallites with sharp boundaries and sizes of 1–10 μm, which is described by the squared Lorentzian function. An additional contribution to the scattering intensity as a result of scattering at an ensemble of defects is found as well, which is characteristic of manganese-rich samples. This contribution is well fitted by the power function Q–n with the exponent n = 3. The complementary scattering typical of iron-rich samples is described by an exponential function and also seems to be a part of scattering at sharp-boundary crystallites.
KW - defects
KW - fractal structure
KW - small-angle neutron scattering
KW - synthesis under high pressure and temperature
KW - transition-metalmonogermanides
UR - http://www.scopus.com/inward/record.url?scp=85087516668&partnerID=8YFLogxK
U2 - 10.1134/S1027451020030209
DO - 10.1134/S1027451020030209
M3 - Article
AN - SCOPUS:85087516668
VL - 14
SP - 429
EP - 433
JO - ПОВЕРХНОСТЬ. РЕНТГЕНОВСКИЕ, СИНХРОТРОННЫЕ И НЕЙТРОННЫЕ ИССЛЕДОВАНИЯ
JF - ПОВЕРХНОСТЬ. РЕНТГЕНОВСКИЕ, СИНХРОТРОННЫЕ И НЕЙТРОННЫЕ ИССЛЕДОВАНИЯ
SN - 1027-4510
IS - 3
ER -
ID: 85653988