Standard

Ni-functionalized submicron mesoporous silica particles as a sorbent for metal affinity chromatography. / Kurdyukov, Dmitry A.; Chernova, Ekaterina N.; Russkikh, Yana V.; Eurov, Daniil A.; Sokolov, Vasily V.; Bykova, Anna A.; Shilovskikh, Vladimir V.; Keltsieva, Olga A.; Ubyivovk, Eugenii V.; Anufrikov, Yuri A.; Fedorova, Anna V.; Selyutin, Artem A.; Sukhodolov, Nicolay G.; Podolskaya, Ekaterina P.; Golubev, Valery G.

в: Journal of Chromatography A, Том 1513, 01.09.2017, стр. 140-148.

Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование

Harvard

Kurdyukov, DA, Chernova, EN, Russkikh, YV, Eurov, DA, Sokolov, VV, Bykova, AA, Shilovskikh, VV, Keltsieva, OA, Ubyivovk, EV, Anufrikov, YA, Fedorova, AV, Selyutin, AA, Sukhodolov, NG, Podolskaya, EP & Golubev, VG 2017, 'Ni-functionalized submicron mesoporous silica particles as a sorbent for metal affinity chromatography', Journal of Chromatography A, Том. 1513, стр. 140-148. https://doi.org/10.1016/j.chroma.2017.07.043

APA

Kurdyukov, D. A., Chernova, E. N., Russkikh, Y. V., Eurov, D. A., Sokolov, V. V., Bykova, A. A., Shilovskikh, V. V., Keltsieva, O. A., Ubyivovk, E. V., Anufrikov, Y. A., Fedorova, A. V., Selyutin, A. A., Sukhodolov, N. G., Podolskaya, E. P., & Golubev, V. G. (2017). Ni-functionalized submicron mesoporous silica particles as a sorbent for metal affinity chromatography. Journal of Chromatography A, 1513, 140-148. https://doi.org/10.1016/j.chroma.2017.07.043

Vancouver

Kurdyukov DA, Chernova EN, Russkikh YV, Eurov DA, Sokolov VV, Bykova AA и пр. Ni-functionalized submicron mesoporous silica particles as a sorbent for metal affinity chromatography. Journal of Chromatography A. 2017 Сент. 1;1513:140-148. https://doi.org/10.1016/j.chroma.2017.07.043

Author

Kurdyukov, Dmitry A. ; Chernova, Ekaterina N. ; Russkikh, Yana V. ; Eurov, Daniil A. ; Sokolov, Vasily V. ; Bykova, Anna A. ; Shilovskikh, Vladimir V. ; Keltsieva, Olga A. ; Ubyivovk, Eugenii V. ; Anufrikov, Yuri A. ; Fedorova, Anna V. ; Selyutin, Artem A. ; Sukhodolov, Nicolay G. ; Podolskaya, Ekaterina P. ; Golubev, Valery G. / Ni-functionalized submicron mesoporous silica particles as a sorbent for metal affinity chromatography. в: Journal of Chromatography A. 2017 ; Том 1513. стр. 140-148.

BibTeX

@article{0896ab320ce34f83aaead081dd0088e6,
title = "Ni-functionalized submicron mesoporous silica particles as a sorbent for metal affinity chromatography",
abstract = "In this research, a novel IMAC sorbent with high specificity for chlorine-containing compounds was developed. Ni-functionalized monodisperse spherical mesoporous silica particles of 500 ± 25 nm diameter were synthesized and their metal affinity properties were studied with the use of diclofenac as the model substance. The particles were aggregatively stable in the pH range of 3–12. The sorbent demonstrated a high adsorption capacity (0.60 ± 0.06 μg of DCF per 1 mg of the sorbent) and high adsorption/desorption rate (20 and 5 min was enough for the sorbent saturation and desorption of DCF, correspondingly). A mixture of eluents with addition of PFOS providing the almost complete recovery (98%) of diclofenac was first proposed. The monodispersity and the high sedimentation and aggregative stability of the particles provide the formation of a stable hydrosol even under ultrasound treatment which makes the mSiO2/Ni particles suitable for batch chromatography.",
keywords = "Affinity sorbent, Fabrication, IMAC, Mesoporous silica particles, Monodispersity, Nickel",
author = "Kurdyukov, {Dmitry A.} and Chernova, {Ekaterina N.} and Russkikh, {Yana V.} and Eurov, {Daniil A.} and Sokolov, {Vasily V.} and Bykova, {Anna A.} and Shilovskikh, {Vladimir V.} and Keltsieva, {Olga A.} and Ubyivovk, {Eugenii V.} and Anufrikov, {Yuri A.} and Fedorova, {Anna V.} and Selyutin, {Artem A.} and Sukhodolov, {Nicolay G.} and Podolskaya, {Ekaterina P.} and Golubev, {Valery G.}",
year = "2017",
month = sep,
day = "1",
doi = "10.1016/j.chroma.2017.07.043",
language = "English",
volume = "1513",
pages = "140--148",
journal = "Journal of Chromatography",
issn = "0021-9673",
publisher = "Elsevier",

}

RIS

TY - JOUR

T1 - Ni-functionalized submicron mesoporous silica particles as a sorbent for metal affinity chromatography

AU - Kurdyukov, Dmitry A.

AU - Chernova, Ekaterina N.

AU - Russkikh, Yana V.

AU - Eurov, Daniil A.

AU - Sokolov, Vasily V.

AU - Bykova, Anna A.

AU - Shilovskikh, Vladimir V.

AU - Keltsieva, Olga A.

AU - Ubyivovk, Eugenii V.

AU - Anufrikov, Yuri A.

AU - Fedorova, Anna V.

AU - Selyutin, Artem A.

AU - Sukhodolov, Nicolay G.

AU - Podolskaya, Ekaterina P.

AU - Golubev, Valery G.

PY - 2017/9/1

Y1 - 2017/9/1

N2 - In this research, a novel IMAC sorbent with high specificity for chlorine-containing compounds was developed. Ni-functionalized monodisperse spherical mesoporous silica particles of 500 ± 25 nm diameter were synthesized and their metal affinity properties were studied with the use of diclofenac as the model substance. The particles were aggregatively stable in the pH range of 3–12. The sorbent demonstrated a high adsorption capacity (0.60 ± 0.06 μg of DCF per 1 mg of the sorbent) and high adsorption/desorption rate (20 and 5 min was enough for the sorbent saturation and desorption of DCF, correspondingly). A mixture of eluents with addition of PFOS providing the almost complete recovery (98%) of diclofenac was first proposed. The monodispersity and the high sedimentation and aggregative stability of the particles provide the formation of a stable hydrosol even under ultrasound treatment which makes the mSiO2/Ni particles suitable for batch chromatography.

AB - In this research, a novel IMAC sorbent with high specificity for chlorine-containing compounds was developed. Ni-functionalized monodisperse spherical mesoporous silica particles of 500 ± 25 nm diameter were synthesized and their metal affinity properties were studied with the use of diclofenac as the model substance. The particles were aggregatively stable in the pH range of 3–12. The sorbent demonstrated a high adsorption capacity (0.60 ± 0.06 μg of DCF per 1 mg of the sorbent) and high adsorption/desorption rate (20 and 5 min was enough for the sorbent saturation and desorption of DCF, correspondingly). A mixture of eluents with addition of PFOS providing the almost complete recovery (98%) of diclofenac was first proposed. The monodispersity and the high sedimentation and aggregative stability of the particles provide the formation of a stable hydrosol even under ultrasound treatment which makes the mSiO2/Ni particles suitable for batch chromatography.

KW - Affinity sorbent

KW - Fabrication

KW - IMAC

KW - Mesoporous silica particles

KW - Monodispersity

KW - Nickel

UR - http://www.scopus.com/inward/record.url?scp=85025428832&partnerID=8YFLogxK

U2 - 10.1016/j.chroma.2017.07.043

DO - 10.1016/j.chroma.2017.07.043

M3 - Article

AN - SCOPUS:85025428832

VL - 1513

SP - 140

EP - 148

JO - Journal of Chromatography

JF - Journal of Chromatography

SN - 0021-9673

ER -

ID: 10084099