Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование
Formation and mechanical properties of alumina ceramics based on Al2O3 micro- and nanoparticles. / Zemtsova, E.G.; Monin, A.V.; Smirnov, V.M.; Semenov, B.N.; Morozov, N.F.
в: Physical Mesomechanics, Том 18, № 2, 2015, стр. 134-138.Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование
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TY - JOUR
T1 - Formation and mechanical properties of alumina ceramics based on Al2O3 micro- and nanoparticles
AU - Zemtsova, E.G.
AU - Monin, A.V.
AU - Smirnov, V.M.
AU - Semenov, B.N.
AU - Morozov, N.F.
PY - 2015
Y1 - 2015
N2 - Alumina micro- and nanopowders with the particle size from 200 mu m to 40 nm synthesized by the sol-gel method are studied. The particle size dependence of gamma-Al2O3 ->alpha-Al2O3 phase transformation is studied by differential thermal analysis, X-ray diffraction method, and transmission electron microscopy. X-ray diffraction data show that for alumina nanoparticles gamma-Al2O3 ->alpha-Al2O3 phase transformation occurs at 900A degrees C, and for micro-particles it occurs in the temperature range 1150-1200A degrees C. The alumina ceramics produced of alumina nanoparticles is shown to have higher flexural strength under three-point bending than the ceramics produced of micro-particles. The obtained results demonstrate that alumina particle size reduction stabilizes the formation of alpha-Al2O3 at lower temperatures, due to which the grain growth rate decreases and the flexural strength of monolithic oxide ceramics increases.
AB - Alumina micro- and nanopowders with the particle size from 200 mu m to 40 nm synthesized by the sol-gel method are studied. The particle size dependence of gamma-Al2O3 ->alpha-Al2O3 phase transformation is studied by differential thermal analysis, X-ray diffraction method, and transmission electron microscopy. X-ray diffraction data show that for alumina nanoparticles gamma-Al2O3 ->alpha-Al2O3 phase transformation occurs at 900A degrees C, and for micro-particles it occurs in the temperature range 1150-1200A degrees C. The alumina ceramics produced of alumina nanoparticles is shown to have higher flexural strength under three-point bending than the ceramics produced of micro-particles. The obtained results demonstrate that alumina particle size reduction stabilizes the formation of alpha-Al2O3 at lower temperatures, due to which the grain growth rate decreases and the flexural strength of monolithic oxide ceramics increases.
U2 - 10.1134/S1029959915020058
DO - 10.1134/S1029959915020058
M3 - Article
VL - 18
SP - 134
EP - 138
JO - Physical Mesomechanics
JF - Physical Mesomechanics
SN - 1029-9599
IS - 2
ER -
ID: 4003641