Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование
Facile synthesis of scandium fluoride oriented single-crystalline rods and urchin-like structures by a gas-solution interface technique. / Gulina, L. B.; Tolstoy, V. P.; Kasatkin, I. A.; Murin, I. V.
в: CrystEngComm, Том 19, № 36, 2017, стр. 5412-5416.Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование
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TY - JOUR
T1 - Facile synthesis of scandium fluoride oriented single-crystalline rods and urchin-like structures by a gas-solution interface technique
AU - Gulina, L. B.
AU - Tolstoy, V. P.
AU - Kasatkin, I. A.
AU - Murin, I. V.
PY - 2017
Y1 - 2017
N2 - A facile and effective method to obtain urchin-like structures and ordered arrays of rod-like crystals of scandium fluoride by an interfacial interaction between solution and gaseous reagents (Gas-Solution Interface Technique, GSIT) is reported. The rod crystals with tetragonal crystal lattice can be as thin as ca. 200 nm and as long as ca. 7 μm. The effect of solution concentration and reaction time on the morphology of the product is reported. The synthesized crystals were characterized by SEM, TEM, HRTEM, XRD analyses, EDS, XPS, and FT-IR spectroscopy. A hypothesis is proposed on the formation of rod crystals during the GSIT process.
AB - A facile and effective method to obtain urchin-like structures and ordered arrays of rod-like crystals of scandium fluoride by an interfacial interaction between solution and gaseous reagents (Gas-Solution Interface Technique, GSIT) is reported. The rod crystals with tetragonal crystal lattice can be as thin as ca. 200 nm and as long as ca. 7 μm. The effect of solution concentration and reaction time on the morphology of the product is reported. The synthesized crystals were characterized by SEM, TEM, HRTEM, XRD analyses, EDS, XPS, and FT-IR spectroscopy. A hypothesis is proposed on the formation of rod crystals during the GSIT process.
UR - http://www.scopus.com/inward/record.url?scp=85029716841&partnerID=8YFLogxK
U2 - 10.1039/c7ce01396e
DO - 10.1039/c7ce01396e
M3 - Article
AN - SCOPUS:85029716841
VL - 19
SP - 5412
EP - 5416
JO - CrystEngComm
JF - CrystEngComm
SN - 1466-8033
IS - 36
ER -
ID: 9422852