The liquid (I)-liquid (II) extraction equilibria in the five-component system fullerene C₆₀-fullerene C₇₀-1,2,4-C ₆H₃Cl₃-C₂H₅OH-H ₂O were studied at 25°C. Isothermal diagrams of distribution of the fullerene components among stratifying liquid phases at a constant content of H₂O were obtained.