Standard

Determination of silicon, phosphorus, iron and aluminum in biodiesel by multicommutated stepwise injection analysis with сlassical least squares method. / Vakh, Christina S.; Bulatov, Andrey V.; Shishov, Andrey Y.; Zabrodin, Andrey V.; Moskvin, Leonid N.

в: Fuel, Том 135, 2014, стр. 198–204.

Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование

Harvard

Vakh, CS, Bulatov, AV, Shishov, AY, Zabrodin, AV & Moskvin, LN 2014, 'Determination of silicon, phosphorus, iron and aluminum in biodiesel by multicommutated stepwise injection analysis with сlassical least squares method', Fuel, Том. 135, стр. 198–204. https://doi.org/DOI: 10.1016/j.fuel.2014.06.059, https://doi.org/10.1016/j.fuel.2014.06.059

APA

Vakh, C. S., Bulatov, A. V., Shishov, A. Y., Zabrodin, A. V., & Moskvin, L. N. (2014). Determination of silicon, phosphorus, iron and aluminum in biodiesel by multicommutated stepwise injection analysis with сlassical least squares method. Fuel, 135, 198–204. https://doi.org/DOI: 10.1016/j.fuel.2014.06.059, https://doi.org/10.1016/j.fuel.2014.06.059

Vancouver

Vakh CS, Bulatov AV, Shishov AY, Zabrodin AV, Moskvin LN. Determination of silicon, phosphorus, iron and aluminum in biodiesel by multicommutated stepwise injection analysis with сlassical least squares method. Fuel. 2014;135:198–204. https://doi.org/DOI: 10.1016/j.fuel.2014.06.059, https://doi.org/10.1016/j.fuel.2014.06.059

Author

Vakh, Christina S. ; Bulatov, Andrey V. ; Shishov, Andrey Y. ; Zabrodin, Andrey V. ; Moskvin, Leonid N. / Determination of silicon, phosphorus, iron and aluminum in biodiesel by multicommutated stepwise injection analysis with сlassical least squares method. в: Fuel. 2014 ; Том 135. стр. 198–204.

BibTeX

@article{7536183554be45a9bf60db09951da511,
title = "Determination of silicon, phosphorus, iron and aluminum in biodiesel by multicommutated stepwise injection analysis with сlassical least squares method",
abstract = "Recently suggested multicommutated stepwise injection analysis (MCSWIA) coupled with classical least squares method (CLS) has been developed for silicon, phosphorus, iron and aluminum determination in biodiesel samples after a microwave digestion. This method allows to carry out four color-forming reactions simultaneously: aluminum (III) and iron (III) with chromazurol S and phosphate and silicate ions with ammonium molybdate, in two mixing chambers which are commutated into MCSWIA manifold. The concentrations of analytes were determined by two data matrixes using CLS method. Each of experimental calibration matrixes for CLS were designed with 10 calibration set solutions of 1-10 mg kg-1 for aluminum and 2-20 mg kg-1 for iron, silicon and phosphorus. The appropriate experimental conditions for microwave digestion and automated MCSWIA spectrophotometric determination of analytes were investigated. Recovery tests show results between 98% and 107% for all type of biodiesel samples. The limits of detection (LOD)",
author = "Vakh, {Christina S.} and Bulatov, {Andrey V.} and Shishov, {Andrey Y.} and Zabrodin, {Andrey V.} and Moskvin, {Leonid N.}",
year = "2014",
doi = "DOI: 10.1016/j.fuel.2014.06.059",
language = "English",
volume = "135",
pages = "198–204",
journal = "Fuel",
issn = "0016-2361",
publisher = "Elsevier",

}

RIS

TY - JOUR

T1 - Determination of silicon, phosphorus, iron and aluminum in biodiesel by multicommutated stepwise injection analysis with сlassical least squares method

AU - Vakh, Christina S.

AU - Bulatov, Andrey V.

AU - Shishov, Andrey Y.

AU - Zabrodin, Andrey V.

AU - Moskvin, Leonid N.

PY - 2014

Y1 - 2014

N2 - Recently suggested multicommutated stepwise injection analysis (MCSWIA) coupled with classical least squares method (CLS) has been developed for silicon, phosphorus, iron and aluminum determination in biodiesel samples after a microwave digestion. This method allows to carry out four color-forming reactions simultaneously: aluminum (III) and iron (III) with chromazurol S and phosphate and silicate ions with ammonium molybdate, in two mixing chambers which are commutated into MCSWIA manifold. The concentrations of analytes were determined by two data matrixes using CLS method. Each of experimental calibration matrixes for CLS were designed with 10 calibration set solutions of 1-10 mg kg-1 for aluminum and 2-20 mg kg-1 for iron, silicon and phosphorus. The appropriate experimental conditions for microwave digestion and automated MCSWIA spectrophotometric determination of analytes were investigated. Recovery tests show results between 98% and 107% for all type of biodiesel samples. The limits of detection (LOD)

AB - Recently suggested multicommutated stepwise injection analysis (MCSWIA) coupled with classical least squares method (CLS) has been developed for silicon, phosphorus, iron and aluminum determination in biodiesel samples after a microwave digestion. This method allows to carry out four color-forming reactions simultaneously: aluminum (III) and iron (III) with chromazurol S and phosphate and silicate ions with ammonium molybdate, in two mixing chambers which are commutated into MCSWIA manifold. The concentrations of analytes were determined by two data matrixes using CLS method. Each of experimental calibration matrixes for CLS were designed with 10 calibration set solutions of 1-10 mg kg-1 for aluminum and 2-20 mg kg-1 for iron, silicon and phosphorus. The appropriate experimental conditions for microwave digestion and automated MCSWIA spectrophotometric determination of analytes were investigated. Recovery tests show results between 98% and 107% for all type of biodiesel samples. The limits of detection (LOD)

U2 - DOI: 10.1016/j.fuel.2014.06.059

DO - DOI: 10.1016/j.fuel.2014.06.059

M3 - Article

VL - 135

SP - 198

EP - 204

JO - Fuel

JF - Fuel

SN - 0016-2361

ER -

ID: 5720822