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(1RS,3SR)-1-(4-Methylbenzyl)-7-phenyl-5-oxa-6-azaspiro[2.4]hept-6-en-4-one. / Титов, Глеб Денисович; Ростовский, Николай Витальевич.

в: MolBank, Том 2024, № 2, M1799, 01.04.2024.

Результаты исследований: Научные публикации в периодических изданияхстатьяРецензирование

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@article{e38f1c34eeda4982961e334370db1170,
title = "(1RS,3SR)-1-(4-Methylbenzyl)-7-phenyl-5-oxa-6-azaspiro[2.4]hept-6-en-4-one",
abstract = "The previously unknown cyclopropane spiro-fused with isoxazol-5-one ((1RS,3SR)-1-(4-methylbenzyl)-7-phenyl-5-oxa-6-azaspiro[2.4]hept-6-en-4-one) was synthesized from benzylideneisoxazol-5-one in 34% yield via double methylene transfer from diazomethane. The structure of the compound was established based on 1H, 13C, and 2D NMR spectroscopy and high-resolution mass spectrometry, and confirmed by X-ray diffraction analysis.",
author = "Титов, {Глеб Денисович} and Ростовский, {Николай Витальевич}",
year = "2024",
month = apr,
day = "1",
doi = "10.3390/M1799",
language = "English",
volume = "2024",
journal = "MolBank",
issn = "1422-8599",
publisher = "MDPI AG",
number = "2",

}

RIS

TY - JOUR

T1 - (1RS,3SR)-1-(4-Methylbenzyl)-7-phenyl-5-oxa-6-azaspiro[2.4]hept-6-en-4-one

AU - Титов, Глеб Денисович

AU - Ростовский, Николай Витальевич

PY - 2024/4/1

Y1 - 2024/4/1

N2 - The previously unknown cyclopropane spiro-fused with isoxazol-5-one ((1RS,3SR)-1-(4-methylbenzyl)-7-phenyl-5-oxa-6-azaspiro[2.4]hept-6-en-4-one) was synthesized from benzylideneisoxazol-5-one in 34% yield via double methylene transfer from diazomethane. The structure of the compound was established based on 1H, 13C, and 2D NMR spectroscopy and high-resolution mass spectrometry, and confirmed by X-ray diffraction analysis.

AB - The previously unknown cyclopropane spiro-fused with isoxazol-5-one ((1RS,3SR)-1-(4-methylbenzyl)-7-phenyl-5-oxa-6-azaspiro[2.4]hept-6-en-4-one) was synthesized from benzylideneisoxazol-5-one in 34% yield via double methylene transfer from diazomethane. The structure of the compound was established based on 1H, 13C, and 2D NMR spectroscopy and high-resolution mass spectrometry, and confirmed by X-ray diffraction analysis.

UR - https://www.mendeley.com/catalogue/09f3fa04-eaff-3dfd-9bed-717212f5831d/

U2 - 10.3390/M1799

DO - 10.3390/M1799

M3 - Article

VL - 2024

JO - MolBank

JF - MolBank

SN - 1422-8599

IS - 2

M1 - M1799

ER -

ID: 119244677