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Taking diazo transfer to water : alpha-diazo carbonyl compounds from in situ generated mesyl azide. / Shevalev, Robert M.; Zhmurov, Petr A.; Dar'in, Dmitry V.; Krasavin, Mikhail.

In: Mendeleev Communications , Vol. 30, No. 3, 2020, p. 372-373.

Research output: Contribution to journal › Article › peer-review

Harvard

Shevalev, RM, Zhmurov, PA, Dar'in, DV & Krasavin, M 2020, 'Taking diazo transfer to water: alpha-diazo carbonyl compounds from in situ generated mesyl azide', Mendeleev Communications , vol. 30, no. 3, pp. 372-373. https://doi.org/10.1016/j.mencom.2020.05.037

APA

Shevalev, R. M., Zhmurov, P. A., Dar'in, D. V., & Krasavin, M. (2020). Taking diazo transfer to water: alpha-diazo carbonyl compounds from in situ generated mesyl azide. Mendeleev Communications , 30(3), 372-373. https://doi.org/10.1016/j.mencom.2020.05.037

Vancouver

Shevalev RM, Zhmurov PA, Dar'in DV, Krasavin M. Taking diazo transfer to water: alpha-diazo carbonyl compounds from in situ generated mesyl azide. Mendeleev Communications . 2020;30(3):372-373. https://doi.org/10.1016/j.mencom.2020.05.037

Author

Shevalev, Robert M. ; Zhmurov, Petr A. ; Dar'in, Dmitry V. ; Krasavin, Mikhail. / Taking diazo transfer to water : alpha-diazo carbonyl compounds from in situ generated mesyl azide. In: Mendeleev Communications . 2020 ; Vol. 30, No. 3. pp. 372-373.

BibTeX

@article{fa2476cb84944b339c2cd2df05042b2a,
title = "Taking diazo transfer to water: alpha-diazo carbonyl compounds from in situ generated mesyl azide",
abstract = "Mesyl azide generated in situ in aqueous medium converted a range of active methylene substrates into the corresponding diazo compounds in good yields and high purity with no need for chromatographic purification. The products thus obtained are suitable for the subsequent RhII-catalyzed O–H insertions with no need for chromatography in the interim.",
keywords = "active methylene compounds, aqueous medium, diazo transfer, in situ generation, mesyl azide, sulfonyl azides, KETONES",
author = "Shevalev, {Robert M.} and Zhmurov, {Petr A.} and Dar'in, {Dmitry V.} and Mikhail Krasavin",
year = "2020",
doi = "10.1016/j.mencom.2020.05.037",
language = "English",
volume = "30",
pages = "372--373",
journal = "Mendeleev Communications",
issn = "0959-9436",
publisher = "Elsevier",
number = "3",

}

RIS

TY - JOUR

T1 - Taking diazo transfer to water

T2 - alpha-diazo carbonyl compounds from in situ generated mesyl azide

AU - Shevalev, Robert M.

AU - Zhmurov, Petr A.

AU - Dar'in, Dmitry V.

AU - Krasavin, Mikhail

PY - 2020

Y1 - 2020

N2 - Mesyl azide generated in situ in aqueous medium converted a range of active methylene substrates into the corresponding diazo compounds in good yields and high purity with no need for chromatographic purification. The products thus obtained are suitable for the subsequent RhII-catalyzed O–H insertions with no need for chromatography in the interim.

AB - Mesyl azide generated in situ in aqueous medium converted a range of active methylene substrates into the corresponding diazo compounds in good yields and high purity with no need for chromatographic purification. The products thus obtained are suitable for the subsequent RhII-catalyzed O–H insertions with no need for chromatography in the interim.

KW - active methylene compounds

KW - aqueous medium

KW - diazo transfer

KW - in situ generation

KW - mesyl azide

KW - sulfonyl azides

KW - KETONES

UR - http://www.scopus.com/inward/record.url?scp=85086132916&partnerID=8YFLogxK

UR - https://www.sciencedirect.com/science/article/abs/pii/S0959943620301504#!

UR - https://www.mendeley.com/catalogue/215f9eec-7219-37ab-9c68-2a2e78829259/

U2 - 10.1016/j.mencom.2020.05.037

DO - 10.1016/j.mencom.2020.05.037

M3 - Article

AN - SCOPUS:85086132916

VL - 30

SP - 372

EP - 373

JO - Mendeleev Communications

JF - Mendeleev Communications

SN - 0959-9436

IS - 3

ER -

ID: 59750682