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Selection of Conditions for Chromatomembrane Gas Extraction at Its Combination with the Gas-Adsorption Preconcentration of Analytes. / Rodinkov, O. V.; Bugaichenko, A. S.; Moskvin, L. N.; Gorbacheva, A. R.; Vagner, E. A.

In: Journal of Analytical Chemistry, Vol. 73, No. 5, 01.05.2018, p. 432-437.

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@article{55aaa1e532b142afae81fc355b3a0364,
title = "Selection of Conditions for Chromatomembrane Gas Extraction at Its Combination with the Gas-Adsorption Preconcentration of Analytes",
abstract = "Optimal conditions (temperature, porous structure and configuration of mass exchange layer in the chromatomembrane cell, and also the direction of water sample and extractant gas flows through it) for the chromatomembrane gas extraction of volatile organic compounds from aqueous solutions in combination with the gas-adsorption preconcentration of the analytes are selected. An analysis scheme based on a combination of these methods and a two-step thermal desorption of analytes ensures the shortening of the preconcentration time by several times compared to the schemes involving traditional bubbling. Metrological characteristics are given and the accuracy of the developed scheme of analysis is proved.",
keywords = "aqueous solutions, chromatomembrane gas extraction, gas chromatographic determination, gas-adsorption preconcentration, thermal desorption, volatile organic compounds",
author = "Rodinkov, {O. V.} and Bugaichenko, {A. S.} and Moskvin, {L. N.} and Gorbacheva, {A. R.} and Vagner, {E. A.}",
year = "2018",
month = may,
day = "1",
doi = "10.1134/S1061934818050106",
language = "English",
volume = "73",
pages = "432--437",
journal = "Journal of Analytical Chemistry",
issn = "1061-9348",
publisher = "МАИК {"}Наука/Интерпериодика{"}",
number = "5",

}

RIS

TY - JOUR

T1 - Selection of Conditions for Chromatomembrane Gas Extraction at Its Combination with the Gas-Adsorption Preconcentration of Analytes

AU - Rodinkov, O. V.

AU - Bugaichenko, A. S.

AU - Moskvin, L. N.

AU - Gorbacheva, A. R.

AU - Vagner, E. A.

PY - 2018/5/1

Y1 - 2018/5/1

N2 - Optimal conditions (temperature, porous structure and configuration of mass exchange layer in the chromatomembrane cell, and also the direction of water sample and extractant gas flows through it) for the chromatomembrane gas extraction of volatile organic compounds from aqueous solutions in combination with the gas-adsorption preconcentration of the analytes are selected. An analysis scheme based on a combination of these methods and a two-step thermal desorption of analytes ensures the shortening of the preconcentration time by several times compared to the schemes involving traditional bubbling. Metrological characteristics are given and the accuracy of the developed scheme of analysis is proved.

AB - Optimal conditions (temperature, porous structure and configuration of mass exchange layer in the chromatomembrane cell, and also the direction of water sample and extractant gas flows through it) for the chromatomembrane gas extraction of volatile organic compounds from aqueous solutions in combination with the gas-adsorption preconcentration of the analytes are selected. An analysis scheme based on a combination of these methods and a two-step thermal desorption of analytes ensures the shortening of the preconcentration time by several times compared to the schemes involving traditional bubbling. Metrological characteristics are given and the accuracy of the developed scheme of analysis is proved.

KW - aqueous solutions

KW - chromatomembrane gas extraction

KW - gas chromatographic determination

KW - gas-adsorption preconcentration

KW - thermal desorption

KW - volatile organic compounds

UR - http://www.scopus.com/inward/record.url?scp=85046339147&partnerID=8YFLogxK

UR - http://www.mendeley.com/research/selection-conditions-chromatomembrane-gas-extraction-combination-gasadsorption-preconcentration-anal

U2 - 10.1134/S1061934818050106

DO - 10.1134/S1061934818050106

M3 - Article

AN - SCOPUS:85046339147

VL - 73

SP - 432

EP - 437

JO - Journal of Analytical Chemistry

JF - Journal of Analytical Chemistry

SN - 1061-9348

IS - 5

ER -

ID: 33849757