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Physicochemical and hydrodynamic aspects of GdFeO3 production using a free impinging-jets method. / Albadi, Y.; Abiev, R. S.; Sirotkin, A. A.; Martinson, K. D.; Chebanenko, M. I.; Nevedomskiy, V. N.; Buryanenko, I. V.; Semenov, V. G.; Popkov, V. I.

In: Chemical Engineering and Processing - Process Intensification, Vol. 166, 108473, 01.09.2021.

Research output: Contribution to journal › Article › peer-review

Harvard

Albadi, Y, Abiev, RS, Sirotkin, AA, Martinson, KD, Chebanenko, MI, Nevedomskiy, VN, Buryanenko, IV, Semenov, VG & Popkov, VI 2021, 'Physicochemical and hydrodynamic aspects of GdFeO3 production using a free impinging-jets method', Chemical Engineering and Processing - Process Intensification, vol. 166, 108473. https://doi.org/10.1016/j.cep.2021.108473

APA

Albadi, Y., Abiev, R. S., Sirotkin, A. A., Martinson, K. D., Chebanenko, M. I., Nevedomskiy, V. N., Buryanenko, I. V., Semenov, V. G., & Popkov, V. I. (2021). Physicochemical and hydrodynamic aspects of GdFeO3 production using a free impinging-jets method. Chemical Engineering and Processing - Process Intensification, 166, [108473]. https://doi.org/10.1016/j.cep.2021.108473

Vancouver

Albadi Y, Abiev RS, Sirotkin AA, Martinson KD, Chebanenko MI, Nevedomskiy VN et al. Physicochemical and hydrodynamic aspects of GdFeO3 production using a free impinging-jets method. Chemical Engineering and Processing - Process Intensification. 2021 Sep 1;166. 108473. https://doi.org/10.1016/j.cep.2021.108473

Author

Albadi, Y. ; Abiev, R. S. ; Sirotkin, A. A. ; Martinson, K. D. ; Chebanenko, M. I. ; Nevedomskiy, V. N. ; Buryanenko, I. V. ; Semenov, V. G. ; Popkov, V. I. / Physicochemical and hydrodynamic aspects of GdFeO3 production using a free impinging-jets method. In: Chemical Engineering and Processing - Process Intensification. 2021 ; Vol. 166.

BibTeX

@article{18b6eba9cf5a4967b071c05042c205ba,
title = "Physicochemical and hydrodynamic aspects of GdFeO3 production using a free impinging-jets method",
abstract = "A free impinging-jets microreactor (FIJMR) was successfully used for the ultrafast co-precipitation of gadolinium and iron(III) hydroxides and subsequent production of fine GdFeO3 nanoparticles via precipitate heat treatment in the air. The effects of the concentration of Gd3+ and Fe3+ ions (c = 0.001-0.1 mol/L), the temperature of the reaction solutions (t = 0-50°C), the flow rate of the solutions (Qj = 100-400 mL/min) and the jets impingement angle (2θ = 90-180°) on the mixing mode and nanoparticle size were comprehensively analyzed. The impact of co-precipitation parameters was discussed in detail from both physicochemical and hydrodynamic points of view. It was shown that the FIJMR co-precipitation resulted in isometric GdFeO3 nanoparticles with variable average size (<D> = 22.8-40.6 nm) and size distribution variance (FWHM = 19.7-32.2 nm). The optimal parameters were found to be c = 0.01 mol/L, t = 0°C, Qj = 200 mL/min and 2θ = 90° and allowed to produce ultrafine GdFeO3 nanoparticles (<D> = 22.8 nm) with narrow size distribution (FWHM = 20.5 nm), unified morphology, high visible-light absorption and superparamagnetic behavior. Based on these results, FIJMR-assisted co-precipitation was concluded to be an efficient and prospective method for the physicochemical design and production of advanced functional nanopowders.",
keywords = "Co-precipitation, Free impinging-jets microreactor, Gadolinium orthoferrite, Material design, Micromixing, Nanoparticles, QUALITY, SIZE, NANOMATERIALS, BARIUM-SULFATE, MICROMIXERS, NANOPARTICLES, PRECIPITATION, MICROREACTORS, LA",
author = "Y. Albadi and Abiev, {R. S.} and Sirotkin, {A. A.} and Martinson, {K. D.} and Chebanenko, {M. I.} and Nevedomskiy, {V. N.} and Buryanenko, {I. V.} and Semenov, {V. G.} and Popkov, {V. I.}",
note = "Publisher Copyright: {\textcopyright} 2021 Elsevier B.V.",
year = "2021",
month = sep,
day = "1",
doi = "10.1016/j.cep.2021.108473",
language = "English",
volume = "166",
journal = "Chemical Engineering and Processing - Process Intensification",
issn = "0255-2701",
publisher = "Elsevier",

}

RIS

TY - JOUR

T1 - Physicochemical and hydrodynamic aspects of GdFeO3 production using a free impinging-jets method

AU - Albadi, Y.

AU - Abiev, R. S.

AU - Sirotkin, A. A.

AU - Martinson, K. D.

AU - Chebanenko, M. I.

AU - Nevedomskiy, V. N.

AU - Buryanenko, I. V.

AU - Semenov, V. G.

AU - Popkov, V. I.

N1 - Publisher Copyright: © 2021 Elsevier B.V.

PY - 2021/9/1

Y1 - 2021/9/1

N2 - A free impinging-jets microreactor (FIJMR) was successfully used for the ultrafast co-precipitation of gadolinium and iron(III) hydroxides and subsequent production of fine GdFeO3 nanoparticles via precipitate heat treatment in the air. The effects of the concentration of Gd3+ and Fe3+ ions (c = 0.001-0.1 mol/L), the temperature of the reaction solutions (t = 0-50°C), the flow rate of the solutions (Qj = 100-400 mL/min) and the jets impingement angle (2θ = 90-180°) on the mixing mode and nanoparticle size were comprehensively analyzed. The impact of co-precipitation parameters was discussed in detail from both physicochemical and hydrodynamic points of view. It was shown that the FIJMR co-precipitation resulted in isometric GdFeO3 nanoparticles with variable average size (<D> = 22.8-40.6 nm) and size distribution variance (FWHM = 19.7-32.2 nm). The optimal parameters were found to be c = 0.01 mol/L, t = 0°C, Qj = 200 mL/min and 2θ = 90° and allowed to produce ultrafine GdFeO3 nanoparticles (<D> = 22.8 nm) with narrow size distribution (FWHM = 20.5 nm), unified morphology, high visible-light absorption and superparamagnetic behavior. Based on these results, FIJMR-assisted co-precipitation was concluded to be an efficient and prospective method for the physicochemical design and production of advanced functional nanopowders.

AB - A free impinging-jets microreactor (FIJMR) was successfully used for the ultrafast co-precipitation of gadolinium and iron(III) hydroxides and subsequent production of fine GdFeO3 nanoparticles via precipitate heat treatment in the air. The effects of the concentration of Gd3+ and Fe3+ ions (c = 0.001-0.1 mol/L), the temperature of the reaction solutions (t = 0-50°C), the flow rate of the solutions (Qj = 100-400 mL/min) and the jets impingement angle (2θ = 90-180°) on the mixing mode and nanoparticle size were comprehensively analyzed. The impact of co-precipitation parameters was discussed in detail from both physicochemical and hydrodynamic points of view. It was shown that the FIJMR co-precipitation resulted in isometric GdFeO3 nanoparticles with variable average size (<D> = 22.8-40.6 nm) and size distribution variance (FWHM = 19.7-32.2 nm). The optimal parameters were found to be c = 0.01 mol/L, t = 0°C, Qj = 200 mL/min and 2θ = 90° and allowed to produce ultrafine GdFeO3 nanoparticles (<D> = 22.8 nm) with narrow size distribution (FWHM = 20.5 nm), unified morphology, high visible-light absorption and superparamagnetic behavior. Based on these results, FIJMR-assisted co-precipitation was concluded to be an efficient and prospective method for the physicochemical design and production of advanced functional nanopowders.

KW - Co-precipitation

KW - Free impinging-jets microreactor

KW - Gadolinium orthoferrite

KW - Material design

KW - Micromixing

KW - Nanoparticles

KW - QUALITY

KW - SIZE

KW - NANOMATERIALS

KW - BARIUM-SULFATE

KW - MICROMIXERS

KW - NANOPARTICLES

KW - PRECIPITATION

KW - MICROREACTORS

KW - LA

UR - http://www.scopus.com/inward/record.url?scp=85107160180&partnerID=8YFLogxK

UR - https://www.mendeley.com/catalogue/2a4220bc-5f8b-36a2-b49f-73ffc0e836f5/

U2 - 10.1016/j.cep.2021.108473

DO - 10.1016/j.cep.2021.108473

M3 - Article

AN - SCOPUS:85107160180

VL - 166

JO - Chemical Engineering and Processing - Process Intensification

JF - Chemical Engineering and Processing - Process Intensification

SN - 0255-2701

M1 - 108473

ER -

ID: 87427620