Phase composition and dispersity of calcia stabilized zirconiaprecursor, obtained from mixed water-7 vol.%acetone solution

Standard

Phase composition and dispersity of calcia stabilized zirconiaprecursor, obtained from mixed water-7 vol.%acetone solution. / Kurapova, O. Yu ; Grega, M. E.; Somova, V. D.; Golubev, S. N.; Konakov, V. G.

In: Reviews on Advanced Materials Science, Vol. 52, No. 1-2, 2017, p. 121-125.

Research output: Contribution to journal › Article › peer-review

BibTeX

@article{0a02203e32074e8fa9ef263c6db7f1cf,

title = "Phase composition and dispersity of calcia stabilized zirconiaprecursor, obtained from mixed water-7 vol.%acetone solution",

abstract = "The work reports the synthesis and of 9CaO-91ZrO2 (mol.%) precursor, synthesized by co-precipitation from mixed water-acetone solution. By SEM and adsorption-desorption analysis it was shown that acetone addition acts as cryoprotectant effectively reducing the growth of large hexagonal ice crystals during freeze-drying and results in microporous flakes-like particles. STA analysis showed the decreased crystallization enthalpy comparing to values for powder, obtained from aqueous solution. For the first time the systematic investigation of thermal evolution of agglomerates, crystallites and phase composition of powder obtained from mixed water-7vol.% acetone solution has been performed via PSD and XRD.",

author = "Kurapova, {O. Yu} and Grega, {M. E.} and Somova, {V. D.} and Golubev, {S. N.} and Konakov, {V. G.}",

year = "2017",

language = "English",

volume = "52",

pages = "121--125",

journal = "Reviews on Advanced Materials Science",

issn = "1606-5131",

publisher = "Институт проблем машиноведения РАН",

number = "1-2",

}

RIS

TY - JOUR

T1 - Phase composition and dispersity of calcia stabilized zirconiaprecursor, obtained from mixed water-7 vol.%acetone solution

AU - Kurapova, O. Yu

AU - Grega, M. E.

AU - Somova, V. D.

AU - Golubev, S. N.

AU - Konakov, V. G.

PY - 2017

Y1 - 2017

N2 - The work reports the synthesis and of 9CaO-91ZrO2 (mol.%) precursor, synthesized by co-precipitation from mixed water-acetone solution. By SEM and adsorption-desorption analysis it was shown that acetone addition acts as cryoprotectant effectively reducing the growth of large hexagonal ice crystals during freeze-drying and results in microporous flakes-like particles. STA analysis showed the decreased crystallization enthalpy comparing to values for powder, obtained from aqueous solution. For the first time the systematic investigation of thermal evolution of agglomerates, crystallites and phase composition of powder obtained from mixed water-7vol.% acetone solution has been performed via PSD and XRD.

AB - The work reports the synthesis and of 9CaO-91ZrO2 (mol.%) precursor, synthesized by co-precipitation from mixed water-acetone solution. By SEM and adsorption-desorption analysis it was shown that acetone addition acts as cryoprotectant effectively reducing the growth of large hexagonal ice crystals during freeze-drying and results in microporous flakes-like particles. STA analysis showed the decreased crystallization enthalpy comparing to values for powder, obtained from aqueous solution. For the first time the systematic investigation of thermal evolution of agglomerates, crystallites and phase composition of powder obtained from mixed water-7vol.% acetone solution has been performed via PSD and XRD.

UR - http://www.scopus.com/inward/record.url?scp=85040014553&partnerID=8YFLogxK

M3 - Article

AN - SCOPUS:85040014553

VL - 52

SP - 121

EP - 125

JO - Reviews on Advanced Materials Science

JF - Reviews on Advanced Materials Science

SN - 1606-5131

IS - 1-2

ER -

ID: 75434296