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Modified synthesis and structural features of 2-benzylidene-4-nitro-2,5-dihydrothiophene 1,1-dioxides. / Savelev, Igor I.; Efremova, Irina E.; Lapshina, Lidiya V.; Gurzhiy, Vladislav V.; Belyakov, Alexander V.

In: Chemistry of Heterocyclic Compounds, Vol. 57, No. 7-8, 08.2021, p. 861-865.

Research output: Contribution to journal › Article › peer-review

Harvard

Savelev, II, Efremova, IE, Lapshina, LV, Gurzhiy, VV & Belyakov, AV 2021, 'Modified synthesis and structural features of 2-benzylidene-4-nitro-2,5-dihydrothiophene 1,1-dioxides', Chemistry of Heterocyclic Compounds, vol. 57, no. 7-8, pp. 861-865. https://doi.org/10.1007/s10593-021-02992-6

APA

Savelev, I. I., Efremova, I. E., Lapshina, L. V., Gurzhiy, V. V., & Belyakov, A. V. (2021). Modified synthesis and structural features of 2-benzylidene-4-nitro-2,5-dihydrothiophene 1,1-dioxides. Chemistry of Heterocyclic Compounds, 57(7-8), 861-865. https://doi.org/10.1007/s10593-021-02992-6

Vancouver

Savelev II, Efremova IE, Lapshina LV, Gurzhiy VV, Belyakov AV. Modified synthesis and structural features of 2-benzylidene-4-nitro-2,5-dihydrothiophene 1,1-dioxides. Chemistry of Heterocyclic Compounds. 2021 Aug;57(7-8):861-865. https://doi.org/10.1007/s10593-021-02992-6

Author

Savelev, Igor I. ; Efremova, Irina E. ; Lapshina, Lidiya V. ; Gurzhiy, Vladislav V. ; Belyakov, Alexander V. / Modified synthesis and structural features of 2-benzylidene-4-nitro-2,5-dihydrothiophene 1,1-dioxides. In: Chemistry of Heterocyclic Compounds. 2021 ; Vol. 57, No. 7-8. pp. 861-865.

BibTeX

@article{9eca6c1254f942a9a23d9a284dd192b5,
title = "Modified synthesis and structural features of 2-benzylidene-4-nitro-2,5-dihydrothiophene 1,1-dioxides",
abstract = "[Figure not available: see fulltext.] A modified procedure for achieving condensation reactions between 3-methyl-4-nitro-2,5-dihydrothiophene 1,1-dioxide and aromatic aldehydes was used to synthesize a broad range of previously unknown 2-benzylidene-4-nitro-2,5-dihydrothiophene 1,1-dioxides – promising substrates for the assembly of fused polycyclic nitrosulfolane derivatives. The structural features of the obtained nitrosulfodienes were established on the basis of IR spectra, 1Н and 13С NMR spectra, two-dimensional 1Н–13С HMQC and 1Н–13С HMBC experiments, quantum-chemical calculations, and X-ray structural analysis.",
keywords = "2-benzylidene-4-nitro-2,5-dihydrothiophene 1,1-dioxides, condensation, modification of reaction conditions, nitrodienes, sulfolenes",
author = "Savelev, {Igor I.} and Efremova, {Irina E.} and Lapshina, {Lidiya V.} and Gurzhiy, {Vladislav V.} and Belyakov, {Alexander V.}",
note = "Publisher Copyright: {\textcopyright} 2021, Springer Science+Business Media, LLC, part of Springer Nature.",
year = "2021",
month = aug,
doi = "10.1007/s10593-021-02992-6",
language = "English",
volume = "57",
pages = "861--865",
journal = "Chemistry of Heterocyclic Compounds",
issn = "0009-3122",
publisher = "Springer Nature",
number = "7-8",

}

RIS

TY - JOUR

T1 - Modified synthesis and structural features of 2-benzylidene-4-nitro-2,5-dihydrothiophene 1,1-dioxides

AU - Savelev, Igor I.

AU - Efremova, Irina E.

AU - Lapshina, Lidiya V.

AU - Gurzhiy, Vladislav V.

AU - Belyakov, Alexander V.

N1 - Publisher Copyright: © 2021, Springer Science+Business Media, LLC, part of Springer Nature.

PY - 2021/8

Y1 - 2021/8

N2 - [Figure not available: see fulltext.] A modified procedure for achieving condensation reactions between 3-methyl-4-nitro-2,5-dihydrothiophene 1,1-dioxide and aromatic aldehydes was used to synthesize a broad range of previously unknown 2-benzylidene-4-nitro-2,5-dihydrothiophene 1,1-dioxides – promising substrates for the assembly of fused polycyclic nitrosulfolane derivatives. The structural features of the obtained nitrosulfodienes were established on the basis of IR spectra, 1Н and 13С NMR spectra, two-dimensional 1Н–13С HMQC and 1Н–13С HMBC experiments, quantum-chemical calculations, and X-ray structural analysis.

AB - [Figure not available: see fulltext.] A modified procedure for achieving condensation reactions between 3-methyl-4-nitro-2,5-dihydrothiophene 1,1-dioxide and aromatic aldehydes was used to synthesize a broad range of previously unknown 2-benzylidene-4-nitro-2,5-dihydrothiophene 1,1-dioxides – promising substrates for the assembly of fused polycyclic nitrosulfolane derivatives. The structural features of the obtained nitrosulfodienes were established on the basis of IR spectra, 1Н and 13С NMR spectra, two-dimensional 1Н–13С HMQC and 1Н–13С HMBC experiments, quantum-chemical calculations, and X-ray structural analysis.

KW - 2-benzylidene-4-nitro-2,5-dihydrothiophene 1,1-dioxides

KW - condensation

KW - modification of reaction conditions

KW - nitrodienes

KW - sulfolenes

UR - http://www.scopus.com/inward/record.url?scp=85114327847&partnerID=8YFLogxK

U2 - 10.1007/s10593-021-02992-6

DO - 10.1007/s10593-021-02992-6

M3 - Article

AN - SCOPUS:85114327847

VL - 57

SP - 861

EP - 865

JO - Chemistry of Heterocyclic Compounds

JF - Chemistry of Heterocyclic Compounds

SN - 0009-3122

IS - 7-8

ER -

ID: 98952755