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Lumas-30 time-of-flight mass spectrometer with pulsed glow discharge for direct determination of nitrogen in steel. / Ganeev, A. A.; Gubal, A. R.; Mosichev, V. I.; Pershin, N. V.; Petrov, S. N.; Potapov, S. V.; Uskov, K. N.

In: Journal of Analytical Chemistry, Vol. 66, No. 14, 01.12.2011, p. 1411-1416.

Research output: Contribution to journal › Article › peer-review

Harvard

Ganeev, AA, Gubal, AR, Mosichev, VI, Pershin, NV, Petrov, SN, Potapov, SV & Uskov, KN 2011, 'Lumas-30 time-of-flight mass spectrometer with pulsed glow discharge for direct determination of nitrogen in steel', Journal of Analytical Chemistry, vol. 66, no. 14, pp. 1411-1416. https://doi.org/10.1134/S1061934811140097

APA

Ganeev, A. A., Gubal, A. R., Mosichev, V. I., Pershin, N. V., Petrov, S. N., Potapov, S. V., & Uskov, K. N. (2011). Lumas-30 time-of-flight mass spectrometer with pulsed glow discharge for direct determination of nitrogen in steel. Journal of Analytical Chemistry, 66(14), 1411-1416. https://doi.org/10.1134/S1061934811140097

Vancouver

Ganeev AA, Gubal AR, Mosichev VI, Pershin NV, Petrov SN, Potapov SV et al. Lumas-30 time-of-flight mass spectrometer with pulsed glow discharge for direct determination of nitrogen in steel. Journal of Analytical Chemistry. 2011 Dec 1;66(14):1411-1416. https://doi.org/10.1134/S1061934811140097

Author

Ganeev, A. A. ; Gubal, A. R. ; Mosichev, V. I. ; Pershin, N. V. ; Petrov, S. N. ; Potapov, S. V. ; Uskov, K. N. / Lumas-30 time-of-flight mass spectrometer with pulsed glow discharge for direct determination of nitrogen in steel. In: Journal of Analytical Chemistry. 2011 ; Vol. 66, No. 14. pp. 1411-1416.

BibTeX

@article{ecab83555e1d4f9eb51c4ccee224530d,
title = "Lumas-30 time-of-flight mass spectrometer with pulsed glow discharge for direct determination of nitrogen in steel",
abstract = "The problem of quantitative determination of nitrogen in steel has become one of the main tasks in modern metallurgy due to the intensive use of nitrogen as an alloy additive. The presence of such additives is known to improve a number of steel characteristics (corrosion resistance, nonmagnetic behavior, strength, etc.). Both direct and indirect analytical methods have many disadvantages and call for revision. The direct technique of nitrogen determination in steel using a a pulsed glow discharge time-of-flight mass spectrometry is proposed in this paper. Successful application of the method for steel samples with different nitrogen concentrations was demonstrated. Dependence of the nitrogen signal intensity as a function of the repelling pulse delay was investigated, and the optimal delay time was obtained. The detection limit of for the proposed method was found to be 0.03%.",
keywords = "Pulsed glow discharge, Time-of-flight mass spectrometry",
author = "Ganeev, {A. A.} and Gubal, {A. R.} and Mosichev, {V. I.} and Pershin, {N. V.} and Petrov, {S. N.} and Potapov, {S. V.} and Uskov, {K. N.}",
year = "2011",
month = dec,
day = "1",
doi = "10.1134/S1061934811140097",
language = "English",
volume = "66",
pages = "1411--1416",
journal = "Journal of Analytical Chemistry",
issn = "1061-9348",
publisher = "МАИК {"}Наука/Интерпериодика{"}",
number = "14",

}

RIS

TY - JOUR

T1 - Lumas-30 time-of-flight mass spectrometer with pulsed glow discharge for direct determination of nitrogen in steel

AU - Ganeev, A. A.

AU - Gubal, A. R.

AU - Mosichev, V. I.

AU - Pershin, N. V.

AU - Petrov, S. N.

AU - Potapov, S. V.

AU - Uskov, K. N.

PY - 2011/12/1

Y1 - 2011/12/1

N2 - The problem of quantitative determination of nitrogen in steel has become one of the main tasks in modern metallurgy due to the intensive use of nitrogen as an alloy additive. The presence of such additives is known to improve a number of steel characteristics (corrosion resistance, nonmagnetic behavior, strength, etc.). Both direct and indirect analytical methods have many disadvantages and call for revision. The direct technique of nitrogen determination in steel using a a pulsed glow discharge time-of-flight mass spectrometry is proposed in this paper. Successful application of the method for steel samples with different nitrogen concentrations was demonstrated. Dependence of the nitrogen signal intensity as a function of the repelling pulse delay was investigated, and the optimal delay time was obtained. The detection limit of for the proposed method was found to be 0.03%.

AB - The problem of quantitative determination of nitrogen in steel has become one of the main tasks in modern metallurgy due to the intensive use of nitrogen as an alloy additive. The presence of such additives is known to improve a number of steel characteristics (corrosion resistance, nonmagnetic behavior, strength, etc.). Both direct and indirect analytical methods have many disadvantages and call for revision. The direct technique of nitrogen determination in steel using a a pulsed glow discharge time-of-flight mass spectrometry is proposed in this paper. Successful application of the method for steel samples with different nitrogen concentrations was demonstrated. Dependence of the nitrogen signal intensity as a function of the repelling pulse delay was investigated, and the optimal delay time was obtained. The detection limit of for the proposed method was found to be 0.03%.

KW - Pulsed glow discharge

KW - Time-of-flight mass spectrometry

UR - http://www.scopus.com/inward/record.url?scp=84855705075&partnerID=8YFLogxK

U2 - 10.1134/S1061934811140097

DO - 10.1134/S1061934811140097

M3 - Article

AN - SCOPUS:84855705075

VL - 66

SP - 1411

EP - 1416

JO - Journal of Analytical Chemistry

JF - Journal of Analytical Chemistry

SN - 1061-9348

IS - 14

ER -

ID: 36362651