Research output: Contribution to journal › Article › peer-review
Interface-Assisted Synthesis of Single-Crystalline ScF3 Microtubes. / Gulina, Larisa B.; Толстой, Валерий Павлович; Petrov, Yuri V.; Данилов, Денис Васильевич.
In: Inorganic Chemistry, Vol. 57, No. 16, 20.08.2018, p. 9779-9781.Research output: Contribution to journal › Article › peer-review
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TY - JOUR
T1 - Interface-Assisted Synthesis of Single-Crystalline ScF3 Microtubes
AU - Gulina, Larisa B.
AU - Толстой, Валерий Павлович
AU - Petrov, Yuri V.
AU - Данилов, Денис Васильевич
PY - 2018/8/20
Y1 - 2018/8/20
N2 - Scandium fluoride (ScF3) microtubes with nanoscale wall thickness were for the first time successfully synthesized by an interface-assisted technique at the surface of a scandium nitrate aqueous solution without the addition of any surfactant as a result of interaction with hydrofluoric acid from the gaseous phase in only 30 min. X-ray diffraction analysis, scanning electron microscopy, helium ionic microscopy, transmission electron microscopy (TEM), and high-resolution TEM (HRTEM) were used to examine the morphology and crystal structure of ScF3 microtubes. The results show that the ScF3 microtube is single-crystalline and has a hexagonal structure. A hypothetical model of thin-walled microtube formation is proposed.
AB - Scandium fluoride (ScF3) microtubes with nanoscale wall thickness were for the first time successfully synthesized by an interface-assisted technique at the surface of a scandium nitrate aqueous solution without the addition of any surfactant as a result of interaction with hydrofluoric acid from the gaseous phase in only 30 min. X-ray diffraction analysis, scanning electron microscopy, helium ionic microscopy, transmission electron microscopy (TEM), and high-resolution TEM (HRTEM) were used to examine the morphology and crystal structure of ScF3 microtubes. The results show that the ScF3 microtube is single-crystalline and has a hexagonal structure. A hypothetical model of thin-walled microtube formation is proposed.
UR - http://www.scopus.com/inward/record.url?scp=85051855804&partnerID=8YFLogxK
U2 - 10.1021/acs.inorgchem.8b01375
DO - 10.1021/acs.inorgchem.8b01375
M3 - Article
AN - SCOPUS:85051855804
VL - 57
SP - 9779
EP - 9781
JO - Inorganic Chemistry
JF - Inorganic Chemistry
SN - 0020-1669
IS - 16
ER -
ID: 34767321