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Facile Access to 2-Selenoxo-1,2,3,4-tetrahydro-4-quinazolinone Scaffolds and Corresponding Diselenides via Cyclization between Methyl Anthranilate and Isoselenocyanates: Synthesis and Structural Features. / Osmanov, Vladimir K.; Chipinsky, Evgeniy V.; Khrustalev, Victor N.; Novikov, Alexander S.; Askerov, Rizvan Kamiloglu; Chizhov, Alexander O.; Borisova, Galina N.; Borisov, Alexander V.; Grishina, Maria M.; Kurasova, Margarita N.; Kirichuk, Anatoly A.; Peregudov, Alexander S.; Kritchenkov, Andreii S.; Tskhovrebov, Alexander G.
In:
Molecules, Vol. 27, No. 18, 5799, 07.09.2022.
Research output: Contribution to journal › Article › peer-review
Harvard
Osmanov, VK, Chipinsky, EV, Khrustalev, VN
, Novikov, AS, Askerov, RK, Chizhov, AO, Borisova, GN, Borisov, AV, Grishina, MM, Kurasova, MN, Kirichuk, AA, Peregudov, AS, Kritchenkov, AS & Tskhovrebov, AG 2022, '
Facile Access to 2-Selenoxo-1,2,3,4-tetrahydro-4-quinazolinone Scaffolds and Corresponding Diselenides via Cyclization between Methyl Anthranilate and Isoselenocyanates: Synthesis and Structural Features',
Molecules, vol. 27, no. 18, 5799.
https://doi.org/10.3390/molecules27185799APA
Osmanov, V. K., Chipinsky, E. V., Khrustalev, V. N.
, Novikov, A. S., Askerov, R. K., Chizhov, A. O., Borisova, G. N., Borisov, A. V., Grishina, M. M., Kurasova, M. N., Kirichuk, A. A., Peregudov, A. S., Kritchenkov, A. S., & Tskhovrebov, A. G. (2022).
Facile Access to 2-Selenoxo-1,2,3,4-tetrahydro-4-quinazolinone Scaffolds and Corresponding Diselenides via Cyclization between Methyl Anthranilate and Isoselenocyanates: Synthesis and Structural Features.
Molecules,
27(18), [5799].
https://doi.org/10.3390/molecules27185799Vancouver
Author
Osmanov, Vladimir K. ; Chipinsky, Evgeniy V. ; Khrustalev, Victor N.
; Novikov, Alexander S. ; Askerov, Rizvan Kamiloglu ; Chizhov, Alexander O. ; Borisova, Galina N. ; Borisov, Alexander V. ; Grishina, Maria M. ; Kurasova, Margarita N. ; Kirichuk, Anatoly A. ; Peregudov, Alexander S. ; Kritchenkov, Andreii S. ; Tskhovrebov, Alexander G. /
Facile Access to 2-Selenoxo-1,2,3,4-tetrahydro-4-quinazolinone Scaffolds and Corresponding Diselenides via Cyclization between Methyl Anthranilate and Isoselenocyanates: Synthesis and Structural Features. In:
Molecules. 2022 ; Vol. 27, No. 18.
BibTeX
@article{2382b8de2bed4ee7aac34b101f23ef91,
title = "Facile Access to 2-Selenoxo-1,2,3,4-tetrahydro-4-quinazolinone Scaffolds and Corresponding Diselenides via Cyclization between Methyl Anthranilate and Isoselenocyanates: Synthesis and Structural Features",
abstract = "A practical method for the synthesis of 2-selenoxo-1,2,3,4-tetrahydro-4-quinazolinone was reported. The latter compounds were found to undergo facile oxidation with H2O2 into corresponding diselenides. Novel organoselenium derivatives were characterized by the 1H, 77Se, and 13C NMR spectroscopies, high-resolution electrospray ionization mass spectrometry, IR, elemental analyses (C, H, N), and X-ray diffraction analysis for several of them. Novel heterocycles exhibited multiple remarkable chalcogen bonding (ChB) interactions in the solid state, which were studied theoretically.",
keywords = "chalcogen bonding, cyclization, heterocycles, isoselenocyanates, quinazolinones, selenium, Organoselenium Compounds, Quinazolinones, Cyclization, ortho-Aminobenzoates, Hydrogen Peroxide, Chalcogens",
author = "Osmanov, {Vladimir K.} and Chipinsky, {Evgeniy V.} and Khrustalev, {Victor N.} and Novikov, {Alexander S.} and Askerov, {Rizvan Kamiloglu} and Chizhov, {Alexander O.} and Borisova, {Galina N.} and Borisov, {Alexander V.} and Grishina, {Maria M.} and Kurasova, {Margarita N.} and Kirichuk, {Anatoly A.} and Peregudov, {Alexander S.} and Kritchenkov, {Andreii S.} and Tskhovrebov, {Alexander G.}",
note = "Publisher Copyright: {\textcopyright} 2022 by the authors.",
year = "2022",
month = sep,
day = "7",
doi = "10.3390/molecules27185799",
language = "English",
volume = "27",
journal = "Molecules",
issn = "1420-3049",
publisher = "MDPI AG",
number = "18",
}
RIS
TY - JOUR
T1 - Facile Access to 2-Selenoxo-1,2,3,4-tetrahydro-4-quinazolinone Scaffolds and Corresponding Diselenides via Cyclization between Methyl Anthranilate and Isoselenocyanates: Synthesis and Structural Features
AU - Osmanov, Vladimir K.
AU - Chipinsky, Evgeniy V.
AU - Khrustalev, Victor N.
AU - Novikov, Alexander S.
AU - Askerov, Rizvan Kamiloglu
AU - Chizhov, Alexander O.
AU - Borisova, Galina N.
AU - Borisov, Alexander V.
AU - Grishina, Maria M.
AU - Kurasova, Margarita N.
AU - Kirichuk, Anatoly A.
AU - Peregudov, Alexander S.
AU - Kritchenkov, Andreii S.
AU - Tskhovrebov, Alexander G.
N1 - Publisher Copyright:
© 2022 by the authors.
PY - 2022/9/7
Y1 - 2022/9/7
N2 - A practical method for the synthesis of 2-selenoxo-1,2,3,4-tetrahydro-4-quinazolinone was reported. The latter compounds were found to undergo facile oxidation with H2O2 into corresponding diselenides. Novel organoselenium derivatives were characterized by the 1H, 77Se, and 13C NMR spectroscopies, high-resolution electrospray ionization mass spectrometry, IR, elemental analyses (C, H, N), and X-ray diffraction analysis for several of them. Novel heterocycles exhibited multiple remarkable chalcogen bonding (ChB) interactions in the solid state, which were studied theoretically.
AB - A practical method for the synthesis of 2-selenoxo-1,2,3,4-tetrahydro-4-quinazolinone was reported. The latter compounds were found to undergo facile oxidation with H2O2 into corresponding diselenides. Novel organoselenium derivatives were characterized by the 1H, 77Se, and 13C NMR spectroscopies, high-resolution electrospray ionization mass spectrometry, IR, elemental analyses (C, H, N), and X-ray diffraction analysis for several of them. Novel heterocycles exhibited multiple remarkable chalcogen bonding (ChB) interactions in the solid state, which were studied theoretically.
KW - chalcogen bonding
KW - cyclization
KW - heterocycles
KW - isoselenocyanates
KW - quinazolinones
KW - selenium
KW - Organoselenium Compounds
KW - Quinazolinones
KW - Cyclization
KW - ortho-Aminobenzoates
KW - Hydrogen Peroxide
KW - Chalcogens
UR - http://www.scopus.com/inward/record.url?scp=85138390563&partnerID=8YFLogxK
UR - https://www.mendeley.com/catalogue/454c62f6-4963-3d27-820f-0d263888cad9/
U2 - 10.3390/molecules27185799
DO - 10.3390/molecules27185799
M3 - Article
C2 - 36144534
AN - SCOPUS:85138390563
VL - 27
JO - Molecules
JF - Molecules
SN - 1420-3049
IS - 18
M1 - 5799
ER -
