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Convenient preparation of (E)-3-arylidene-4-diazopyrrolidine-2,5-diones in array format. / Chupakhin, Evgeny G.; Kantin, Grigory P.; Dar'in, Dmitry V.; Krasavin, Mikhail.

In: Mendeleev Communications , Vol. 31, No. 1, 01.01.2021, p. 36-38.

Research output: Contribution to journal › Article › peer-review

Harvard

Chupakhin, EG, Kantin, GP, Dar'in, DV & Krasavin, M 2021, 'Convenient preparation of (E)-3-arylidene-4-diazopyrrolidine-2,5-diones in array format', Mendeleev Communications , vol. 31, no. 1, pp. 36-38. https://doi.org/10.1016/j.mencom.2021.01.010

APA

Chupakhin, E. G., Kantin, G. P., Dar'in, D. V., & Krasavin, M. (2021). Convenient preparation of (E)-3-arylidene-4-diazopyrrolidine-2,5-diones in array format. Mendeleev Communications , 31(1), 36-38. https://doi.org/10.1016/j.mencom.2021.01.010

Vancouver

Chupakhin EG, Kantin GP, Dar'in DV, Krasavin M. Convenient preparation of (E)-3-arylidene-4-diazopyrrolidine-2,5-diones in array format. Mendeleev Communications . 2021 Jan 1;31(1):36-38. https://doi.org/10.1016/j.mencom.2021.01.010

Author

Chupakhin, Evgeny G. ; Kantin, Grigory P. ; Dar'in, Dmitry V. ; Krasavin, Mikhail. / Convenient preparation of (E)-3-arylidene-4-diazopyrrolidine-2,5-diones in array format. In: Mendeleev Communications . 2021 ; Vol. 31, No. 1. pp. 36-38.

BibTeX

@article{ba710cd24b0344e7b4cc0e4eece78d61,
title = "Convenient preparation of (E)-3-arylidene-4-diazopyrrolidine-2,5-diones in array format",
abstract = "A practically convenient synthesis of (E)-3-arylidene-4-diazopyrrolidine-2,5-diones from N-substituted maleimides via the Wittig reaction and the Regitz diazo transfer has been developed. In all 26 cases studied, only one chromatographic purification was required with no need for aqueous workup, which makes this protocol amenable to producing the emerging class of diazo compounds in parallel format.",
keywords = "diazo compounds, diazo transfer, maleimides, Michael acceptors, parallel synthesis, privileged structures, Wittig reaction",
author = "Chupakhin, {Evgeny G.} and Kantin, {Grigory P.} and Dar'in, {Dmitry V.} and Mikhail Krasavin",
note = "Funding Information: This research was supported by the Russian Science Foundation (project grant no. 20-13-00024). We thank the Research Center for Magnetic Resonance, the Center for Chemical Analysis and Materials Research and the Center for X-ray Diffraction Methods of Saint Petersburg State University Research Park for obtaining the analytical data. Publisher Copyright: {\textcopyright} 2021 Copyright: Copyright 2021 Elsevier B.V., All rights reserved.",
year = "2021",
month = jan,
day = "1",
doi = "10.1016/j.mencom.2021.01.010",
language = "English",
volume = "31",
pages = "36--38",
journal = "Mendeleev Communications",
issn = "0959-9436",
publisher = "Elsevier",
number = "1",

}

RIS

TY - JOUR

T1 - Convenient preparation of (E)-3-arylidene-4-diazopyrrolidine-2,5-diones in array format

AU - Chupakhin, Evgeny G.

AU - Kantin, Grigory P.

AU - Dar'in, Dmitry V.

AU - Krasavin, Mikhail

N1 - Funding Information: This research was supported by the Russian Science Foundation (project grant no. 20-13-00024). We thank the Research Center for Magnetic Resonance, the Center for Chemical Analysis and Materials Research and the Center for X-ray Diffraction Methods of Saint Petersburg State University Research Park for obtaining the analytical data. Publisher Copyright: © 2021 Copyright: Copyright 2021 Elsevier B.V., All rights reserved.

PY - 2021/1/1

Y1 - 2021/1/1

N2 - A practically convenient synthesis of (E)-3-arylidene-4-diazopyrrolidine-2,5-diones from N-substituted maleimides via the Wittig reaction and the Regitz diazo transfer has been developed. In all 26 cases studied, only one chromatographic purification was required with no need for aqueous workup, which makes this protocol amenable to producing the emerging class of diazo compounds in parallel format.

AB - A practically convenient synthesis of (E)-3-arylidene-4-diazopyrrolidine-2,5-diones from N-substituted maleimides via the Wittig reaction and the Regitz diazo transfer has been developed. In all 26 cases studied, only one chromatographic purification was required with no need for aqueous workup, which makes this protocol amenable to producing the emerging class of diazo compounds in parallel format.

KW - diazo compounds

KW - diazo transfer

KW - maleimides

KW - Michael acceptors

KW - parallel synthesis

KW - privileged structures

KW - Wittig reaction

UR - http://www.scopus.com/inward/record.url?scp=85100701076&partnerID=8YFLogxK

U2 - 10.1016/j.mencom.2021.01.010

DO - 10.1016/j.mencom.2021.01.010

M3 - Article

AN - SCOPUS:85100701076

VL - 31

SP - 36

EP - 38

JO - Mendeleev Communications

JF - Mendeleev Communications

SN - 0959-9436

IS - 1

ER -

ID: 74420724