Research output: Contribution to journal › Article › peer-review
Ceramics of the Cs2O-Al2O3 system prepared by Solid-Phase Technology and the Glycine-Nitrate Combustion Process. / Столярова, Валентина Леонидовна; Федорова, Анна Викторовна; Столяров, Василий Александрович; Павелина, Мария Евгеньевна; Колоницкий, Петр Дмитриевич; Кириченко, С.О.; Тимчук, Андрей Владиславович.
In: Russian Journal of Inorganic Chemistry, Vol. 68, No. 7, 29.09.2023, p. 883-894.Research output: Contribution to journal › Article › peer-review
}
TY - JOUR
T1 - Ceramics of the Cs2O-Al2O3 system prepared by Solid-Phase Technology and the Glycine-Nitrate Combustion Process
AU - Столярова, Валентина Леонидовна
AU - Федорова, Анна Викторовна
AU - Столяров, Василий Александрович
AU - Павелина, Мария Евгеньевна
AU - Колоницкий, Петр Дмитриевич
AU - Кириченко, С.О.
AU - Тимчук, Андрей Владиславович
PY - 2023/9/29
Y1 - 2023/9/29
N2 - Abstract: Cs2O–Al2O3 ceramic samples containing 20 and 33 mol % cesium oxide were prepared by сeramic technique and by the glycine–nitrate combustion process. The prepared samples were identified and characterized by X-ray powder diffraction and X-ray fluorescence analyses, scanning electron microscopy, and differential thermal analysis. X-ray powder diffraction and scanning electron microscopy showed that the phase composition and surface of the samples change significantly and nonmonotonically depending on the synthetic method used and the heat treatment parameters of the batch. Optimal synthetic conditions and heat treatment parameters for preparing Cs2O–Al2O3 samples were elucidated.
AB - Abstract: Cs2O–Al2O3 ceramic samples containing 20 and 33 mol % cesium oxide were prepared by сeramic technique and by the glycine–nitrate combustion process. The prepared samples were identified and characterized by X-ray powder diffraction and X-ray fluorescence analyses, scanning electron microscopy, and differential thermal analysis. X-ray powder diffraction and scanning electron microscopy showed that the phase composition and surface of the samples change significantly and nonmonotonically depending on the synthetic method used and the heat treatment parameters of the batch. Optimal synthetic conditions and heat treatment parameters for preparing Cs2O–Al2O3 samples were elucidated.
UR - https://www.mendeley.com/catalogue/e6f00d16-1889-3e51-8bcd-cee65cd2d783/
U2 - 10.1134/s0036023623600909
DO - 10.1134/s0036023623600909
M3 - Article
VL - 68
SP - 883
EP - 894
JO - Russian Journal of Inorganic Chemistry
JF - Russian Journal of Inorganic Chemistry
SN - 0036-0236
IS - 7
ER -
ID: 105779567