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A new approach for microextraction of non-steroidal anti-inflammatory drugs from human urine samples based on in-situ deep eutectic mixture formation. / Shishov, A. Y.; Chislov, M. V.; Nechaeva, D. V.; Moskvin, L. N.; Bulatov, A. V.

In: Journal of Molecular Liquids, Vol. 272, 15.12.2018, p. 738-745.

Research output: Contribution to journal › Article › peer-review

Harvard

Shishov, AY, Chislov, MV, Nechaeva, DV, Moskvin, LN & Bulatov, AV 2018, 'A new approach for microextraction of non-steroidal anti-inflammatory drugs from human urine samples based on in-situ deep eutectic mixture formation', Journal of Molecular Liquids, vol. 272, pp. 738-745. https://doi.org/10.1016/j.molliq.2018.10.006

APA

Shishov, A. Y., Chislov, M. V., Nechaeva, D. V., Moskvin, L. N., & Bulatov, A. V. (2018). A new approach for microextraction of non-steroidal anti-inflammatory drugs from human urine samples based on in-situ deep eutectic mixture formation. Journal of Molecular Liquids, 272, 738-745. https://doi.org/10.1016/j.molliq.2018.10.006

Vancouver

Shishov AY, Chislov MV, Nechaeva DV, Moskvin LN, Bulatov AV. A new approach for microextraction of non-steroidal anti-inflammatory drugs from human urine samples based on in-situ deep eutectic mixture formation. Journal of Molecular Liquids. 2018 Dec 15;272:738-745. https://doi.org/10.1016/j.molliq.2018.10.006

Author

Shishov, A. Y. ; Chislov, M. V. ; Nechaeva, D. V. ; Moskvin, L. N. ; Bulatov, A. V. / A new approach for microextraction of non-steroidal anti-inflammatory drugs from human urine samples based on in-situ deep eutectic mixture formation. In: Journal of Molecular Liquids. 2018 ; Vol. 272. pp. 738-745.

BibTeX

@article{cd3281de41a24368b9a031a741950119,
title = "A new approach for microextraction of non-steroidal anti-inflammatory drugs from human urine samples based on in-situ deep eutectic mixture formation",
abstract = "A new strategy for the simple, environmental-friendly and highly-available microextraction of non-steroidal anti-inflammatory drugs (NSAIDs) from human urine samples has been proposed. The procedure assumes NSAIDs separation from aqueous sample phase via in-situ forming deep eutectic mixtures based on the formation of hydrogen bond between –OH group of menthol and the oxygen atom of –COOH group of NSAIDs. The developed strategy was used for the HPLC-UV determination of ketoprofen and diclofenac in human urine samples. Under optimal experimental conditions limits of detection, calculated from a blank test, based on 3σ were found to be 15 μg L−1 and 44 μg L−1 for ketoprofen and diclofenac, respectively. The microextraction process can reach equilibrium within 1 min with extraction recovery values from 93 to 97% for both analytes.",
keywords = "Deep eutectic solvent, HPLC-UV, Human urine, Ketoprofen and diclofenac, Menthol, Microextraction, SOLID-PHASE MICROEXTRACTION, CHROMATOGRAPHY, PHARMACEUTICAL FORMULATIONS, EXTRACTION, PLASMA, SOLVENTS, LIQUID-LIQUID MICROEXTRACTION, MENTHOL, HPLC",
author = "Shishov, {A. Y.} and Chislov, {M. V.} and Nechaeva, {D. V.} and Moskvin, {L. N.} and Bulatov, {A. V.}",
year = "2018",
month = dec,
day = "15",
doi = "10.1016/j.molliq.2018.10.006",
language = "English",
volume = "272",
pages = "738--745",
journal = "Journal of Molecular Liquids",
issn = "0167-7322",
publisher = "Elsevier",

}

RIS

TY - JOUR

T1 - A new approach for microextraction of non-steroidal anti-inflammatory drugs from human urine samples based on in-situ deep eutectic mixture formation

AU - Shishov, A. Y.

AU - Chislov, M. V.

AU - Nechaeva, D. V.

AU - Moskvin, L. N.

AU - Bulatov, A. V.

PY - 2018/12/15

Y1 - 2018/12/15

N2 - A new strategy for the simple, environmental-friendly and highly-available microextraction of non-steroidal anti-inflammatory drugs (NSAIDs) from human urine samples has been proposed. The procedure assumes NSAIDs separation from aqueous sample phase via in-situ forming deep eutectic mixtures based on the formation of hydrogen bond between –OH group of menthol and the oxygen atom of –COOH group of NSAIDs. The developed strategy was used for the HPLC-UV determination of ketoprofen and diclofenac in human urine samples. Under optimal experimental conditions limits of detection, calculated from a blank test, based on 3σ were found to be 15 μg L−1 and 44 μg L−1 for ketoprofen and diclofenac, respectively. The microextraction process can reach equilibrium within 1 min with extraction recovery values from 93 to 97% for both analytes.

AB - A new strategy for the simple, environmental-friendly and highly-available microextraction of non-steroidal anti-inflammatory drugs (NSAIDs) from human urine samples has been proposed. The procedure assumes NSAIDs separation from aqueous sample phase via in-situ forming deep eutectic mixtures based on the formation of hydrogen bond between –OH group of menthol and the oxygen atom of –COOH group of NSAIDs. The developed strategy was used for the HPLC-UV determination of ketoprofen and diclofenac in human urine samples. Under optimal experimental conditions limits of detection, calculated from a blank test, based on 3σ were found to be 15 μg L−1 and 44 μg L−1 for ketoprofen and diclofenac, respectively. The microextraction process can reach equilibrium within 1 min with extraction recovery values from 93 to 97% for both analytes.

KW - Deep eutectic solvent

KW - HPLC-UV

KW - Human urine

KW - Ketoprofen and diclofenac

KW - Menthol

KW - Microextraction

KW - SOLID-PHASE MICROEXTRACTION

KW - CHROMATOGRAPHY

KW - PHARMACEUTICAL FORMULATIONS

KW - EXTRACTION

KW - PLASMA

KW - SOLVENTS

KW - LIQUID-LIQUID MICROEXTRACTION

KW - MENTHOL

KW - HPLC

UR - http://www.scopus.com/inward/record.url?scp=85054322244&partnerID=8YFLogxK

U2 - 10.1016/j.molliq.2018.10.006

DO - 10.1016/j.molliq.2018.10.006

M3 - Article

AN - SCOPUS:85054322244

VL - 272

SP - 738

EP - 745

JO - Journal of Molecular Liquids

JF - Journal of Molecular Liquids

SN - 0167-7322

ER -

ID: 36819192