Synthesis and Characterization of Barium Amidoborane

Результат исследований: Научные публикации в периодических изданияхписьмо/краткое сообщениенаучнаярецензирование

Выдержка

Barium amidoborane was synthesized for the first time by the reaction of metal barium with ammonia borane. The compound was characterized by the methods of the solid-phase 11B NMR and IR spectroscopy and elemental analysis. It was shown by simultaneous thermal analysis that hydrogen is the only volatile product of barium amidoborane decomposition in the temperature range 50–240°C.

Язык оригиналаанглийский
Страницы (с-по)2875-2877
Число страниц3
ЖурналRussian Journal of General Chemistry
Том87
Номер выпуска12
DOI
СостояниеОпубликовано - 1 дек 2017

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abstract = "Barium amidoborane was synthesized for the first time by the reaction of metal barium with ammonia borane. The compound was characterized by the methods of the solid-phase 11B NMR and IR spectroscopy and elemental analysis. It was shown by simultaneous thermal analysis that hydrogen is the only volatile product of barium amidoborane decomposition in the temperature range 50–240°C.",
keywords = "amidoboranes, barium, IR spectroscopy, NMR spectroscopy",
author = "Shcherbina, {N. A.} and Kazakov, {I. V.} and Timoshkin, {A. Yu}",
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Synthesis and Characterization of Barium Amidoborane. / Shcherbina, N. A.; Kazakov, I. V.; Timoshkin, A. Yu.

В: Russian Journal of General Chemistry, Том 87, № 12, 01.12.2017, стр. 2875-2877.

Результат исследований: Научные публикации в периодических изданияхписьмо/краткое сообщениенаучнаярецензирование

TY - JOUR

T1 - Synthesis and Characterization of Barium Amidoborane

AU - Shcherbina, N. A.

AU - Kazakov, I. V.

AU - Timoshkin, A. Yu

PY - 2017/12/1

Y1 - 2017/12/1

N2 - Barium amidoborane was synthesized for the first time by the reaction of metal barium with ammonia borane. The compound was characterized by the methods of the solid-phase 11B NMR and IR spectroscopy and elemental analysis. It was shown by simultaneous thermal analysis that hydrogen is the only volatile product of barium amidoborane decomposition in the temperature range 50–240°C.

AB - Barium amidoborane was synthesized for the first time by the reaction of metal barium with ammonia borane. The compound was characterized by the methods of the solid-phase 11B NMR and IR spectroscopy and elemental analysis. It was shown by simultaneous thermal analysis that hydrogen is the only volatile product of barium amidoborane decomposition in the temperature range 50–240°C.

KW - amidoboranes

KW - barium

KW - IR spectroscopy

KW - NMR spectroscopy

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U2 - 10.1134/S1070363217120192

DO - 10.1134/S1070363217120192

M3 - Letter

VL - 87

SP - 2875

EP - 2877

JO - Russian Journal of General Chemistry

JF - Russian Journal of General Chemistry

SN - 1070-3632

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