Lignin Content in Paper Fibers Assessed Using IR Reflectance Spectroscopy

O. Yu Derkacheva, D. O. Tsypkin

Результат исследований: Научные публикации в периодических изданияхстатьянаучная

1 цитирование (Scopus)

Выдержка

A rapid method for analyzing lignin in paper using IR reflectance spectra from its surface was developed. IR absorption and reflectance spectra of model paper samples prepared from cellulose fibers obtained from deciduous and coniferous woods with various lignin contents were analyzed. The intensity of the lignin absorption band at 1510 cm–1 after Kubelka–Munk transformation of the paper reflectance spectra and chemical data on the fiber lignin content were well correlated. The analytical relationship between the lignin content in the paper fibers and the intensity of the lignin absorption band was used to estimate the lignin concentration in samples of Russian stamping paper from the 19th century using their IR reflectance spectra. The cellulose structure parameter estimated from the paper reflectance spectra showed that sheets containing lignin (5–16%) consisted entirely of wood fibers and were supplemented with kaolin.

Язык оригиналаанглийский
Страницы (с-по)1066-1071
Число страниц6
ЖурналJournal of Applied Spectroscopy
Том84
Номер выпуска6
DOI
СостояниеОпубликовано - 1 янв 2018

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    Предметные области Scopus

    • Физика конденсатов
    • Спектроскопия

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    abstract = "A rapid method for analyzing lignin in paper using IR reflectance spectra from its surface was developed. IR absorption and reflectance spectra of model paper samples prepared from cellulose fibers obtained from deciduous and coniferous woods with various lignin contents were analyzed. The intensity of the lignin absorption band at 1510 cm–1 after Kubelka–Munk transformation of the paper reflectance spectra and chemical data on the fiber lignin content were well correlated. The analytical relationship between the lignin content in the paper fibers and the intensity of the lignin absorption band was used to estimate the lignin concentration in samples of Russian stamping paper from the 19th century using their IR reflectance spectra. The cellulose structure parameter estimated from the paper reflectance spectra showed that sheets containing lignin (5–16{\%}) consisted entirely of wood fibers and were supplemented with kaolin.",
    keywords = "analytical dependence, cellulose structure, IR reflectance spectra, kaolin, lignin content, paper",
    author = "Derkacheva, {O. Yu} and Tsypkin, {D. O.}",
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    Lignin Content in Paper Fibers Assessed Using IR Reflectance Spectroscopy. / Derkacheva, O. Yu; Tsypkin, D. O.

    В: Journal of Applied Spectroscopy, Том 84, № 6, 01.01.2018, стр. 1066-1071.

    Результат исследований: Научные публикации в периодических изданияхстатьянаучная

    TY - JOUR

    T1 - Lignin Content in Paper Fibers Assessed Using IR Reflectance Spectroscopy

    AU - Derkacheva, O. Yu

    AU - Tsypkin, D. O.

    PY - 2018/1/1

    Y1 - 2018/1/1

    N2 - A rapid method for analyzing lignin in paper using IR reflectance spectra from its surface was developed. IR absorption and reflectance spectra of model paper samples prepared from cellulose fibers obtained from deciduous and coniferous woods with various lignin contents were analyzed. The intensity of the lignin absorption band at 1510 cm–1 after Kubelka–Munk transformation of the paper reflectance spectra and chemical data on the fiber lignin content were well correlated. The analytical relationship between the lignin content in the paper fibers and the intensity of the lignin absorption band was used to estimate the lignin concentration in samples of Russian stamping paper from the 19th century using their IR reflectance spectra. The cellulose structure parameter estimated from the paper reflectance spectra showed that sheets containing lignin (5–16%) consisted entirely of wood fibers and were supplemented with kaolin.

    AB - A rapid method for analyzing lignin in paper using IR reflectance spectra from its surface was developed. IR absorption and reflectance spectra of model paper samples prepared from cellulose fibers obtained from deciduous and coniferous woods with various lignin contents were analyzed. The intensity of the lignin absorption band at 1510 cm–1 after Kubelka–Munk transformation of the paper reflectance spectra and chemical data on the fiber lignin content were well correlated. The analytical relationship between the lignin content in the paper fibers and the intensity of the lignin absorption band was used to estimate the lignin concentration in samples of Russian stamping paper from the 19th century using their IR reflectance spectra. The cellulose structure parameter estimated from the paper reflectance spectra showed that sheets containing lignin (5–16%) consisted entirely of wood fibers and were supplemented with kaolin.

    KW - analytical dependence

    KW - cellulose structure

    KW - IR reflectance spectra

    KW - kaolin

    KW - lignin content

    KW - paper

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    U2 - 10.1007/s10812-018-0588-6

    DO - 10.1007/s10812-018-0588-6

    M3 - Article

    VL - 84

    SP - 1066

    EP - 1071

    JO - Journal of Applied Spectroscopy (English Translation of Zhurnal Prikladnoi Spektroskopii)

    JF - Journal of Applied Spectroscopy (English Translation of Zhurnal Prikladnoi Spektroskopii)

    SN - 0021-9037

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