Variations in martensitic transformation parameters due to grains evolution during post-deformation heating of Ti-50.2 at. % Ni alloy amorphized by HPT

Natalia Resnina, Sergey Belyaev, Vitali Zeldovich, Vitaly Pilyugin, Natalia Frolova, Diana Glazova

Research output: Contribution to journalArticleResearchpeer-review

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Abstract

The structure and martensitic transformations in Ti-50.2 at. % Ni alloy subjected to high-pressure torsion (HPT) and post-deformation heating were studied. It was shown that HPT under 8GPa for 3.5 turns resulted in an amorphization of the alloy structure but the crystalline debris remained. Further heating of the sample led to alloy crystallization and the bimodal grain size structure formed. The first group of grains underwent a B2  R transition when the average grain size was varied from 20 to 50 nm, and a B2 RB19’I transformations when the average grain size was 80 nm or more. The second group of grains underwent a B2  B19’II transformation. An increase in temperature of amorphous sample heating led to a rise in grain size and as a result, the temperatures of the martensitic transformations changed. The temperatures of the B19’I  B2 transformation and the B2  R transition increased when the heating temperature changed from 359 to 550 oC whereas, the temperatures of the B2  B19’II transformation increased if the amorphous sample was subjected to heating from 415 to 550 oC when the recrystallization took place. It was assumed that the bimodal grain distribution was caused by the grain appeared during crystallization in two ways: from the amorphous phase and from the debris remained in the amorphous phase after HPT.
Original languageEnglish
Pages (from-to)20-30
Number of pages11
JournalThermochimica Acta
Volume627-629
DOIs
StatePublished - 2016

Scopus subject areas

  • Metals and Alloys
  • Materials Science(all)

Cite this

@article{f685545059ea428f8401e35a7421e773,
title = "Variations in martensitic transformation parameters due to grains evolution during post-deformation heating of Ti-50.2 at. {\%} Ni alloy amorphized by HPT",
abstract = "The structure and martensitic transformations in Ti-50.2 at. {\%} Ni alloy subjected to high-pressure torsion (HPT) and post-deformation heating were studied. It was shown that HPT under 8GPa for 3.5 turns resulted in an amorphization of the alloy structure but the crystalline debris remained. Further heating of the sample led to alloy crystallization and the bimodal grain size structure formed. The first group of grains underwent a B2  R transition when the average grain size was varied from 20 to 50 nm, and a B2 RB19’I transformations when the average grain size was 80 nm or more. The second group of grains underwent a B2  B19’II transformation. An increase in temperature of amorphous sample heating led to a rise in grain size and as a result, the temperatures of the martensitic transformations changed. The temperatures of the B19’I  B2 transformation and the B2  R transition increased when the heating temperature changed from 359 to 550 oC whereas, the temperatures of the B2  B19’II transformation increased if the amorphous sample was subjected to heating from 415 to 550 oC when the recrystallization took place. It was assumed that the bimodal grain distribution was caused by the grain appeared during crystallization in two ways: from the amorphous phase and from the debris remained in the amorphous phase after HPT.",
author = "Natalia Resnina and Sergey Belyaev and Vitali Zeldovich and Vitaly Pilyugin and Natalia Frolova and Diana Glazova",
year = "2016",
doi = "10.1016/j.tca.2016.01.015",
language = "English",
volume = "627-629",
pages = "20--30",
journal = "Thermochimica Acta",
issn = "0040-6031",
publisher = "Elsevier",

}

Variations in martensitic transformation parameters due to grains evolution during post-deformation heating of Ti-50.2 at. % Ni alloy amorphized by HPT. / Resnina, Natalia; Belyaev, Sergey; Zeldovich, Vitali; Pilyugin, Vitaly; Frolova, Natalia; Glazova, Diana.

In: Thermochimica Acta, Vol. 627-629, 2016, p. 20-30.

Research output: Contribution to journalArticleResearchpeer-review

TY - JOUR

T1 - Variations in martensitic transformation parameters due to grains evolution during post-deformation heating of Ti-50.2 at. % Ni alloy amorphized by HPT

AU - Resnina, Natalia

AU - Belyaev, Sergey

AU - Zeldovich, Vitali

AU - Pilyugin, Vitaly

AU - Frolova, Natalia

AU - Glazova, Diana

PY - 2016

Y1 - 2016

N2 - The structure and martensitic transformations in Ti-50.2 at. % Ni alloy subjected to high-pressure torsion (HPT) and post-deformation heating were studied. It was shown that HPT under 8GPa for 3.5 turns resulted in an amorphization of the alloy structure but the crystalline debris remained. Further heating of the sample led to alloy crystallization and the bimodal grain size structure formed. The first group of grains underwent a B2  R transition when the average grain size was varied from 20 to 50 nm, and a B2 RB19’I transformations when the average grain size was 80 nm or more. The second group of grains underwent a B2  B19’II transformation. An increase in temperature of amorphous sample heating led to a rise in grain size and as a result, the temperatures of the martensitic transformations changed. The temperatures of the B19’I  B2 transformation and the B2  R transition increased when the heating temperature changed from 359 to 550 oC whereas, the temperatures of the B2  B19’II transformation increased if the amorphous sample was subjected to heating from 415 to 550 oC when the recrystallization took place. It was assumed that the bimodal grain distribution was caused by the grain appeared during crystallization in two ways: from the amorphous phase and from the debris remained in the amorphous phase after HPT.

AB - The structure and martensitic transformations in Ti-50.2 at. % Ni alloy subjected to high-pressure torsion (HPT) and post-deformation heating were studied. It was shown that HPT under 8GPa for 3.5 turns resulted in an amorphization of the alloy structure but the crystalline debris remained. Further heating of the sample led to alloy crystallization and the bimodal grain size structure formed. The first group of grains underwent a B2  R transition when the average grain size was varied from 20 to 50 nm, and a B2 RB19’I transformations when the average grain size was 80 nm or more. The second group of grains underwent a B2  B19’II transformation. An increase in temperature of amorphous sample heating led to a rise in grain size and as a result, the temperatures of the martensitic transformations changed. The temperatures of the B19’I  B2 transformation and the B2  R transition increased when the heating temperature changed from 359 to 550 oC whereas, the temperatures of the B2  B19’II transformation increased if the amorphous sample was subjected to heating from 415 to 550 oC when the recrystallization took place. It was assumed that the bimodal grain distribution was caused by the grain appeared during crystallization in two ways: from the amorphous phase and from the debris remained in the amorphous phase after HPT.

U2 - 10.1016/j.tca.2016.01.015

DO - 10.1016/j.tca.2016.01.015

M3 - Article

VL - 627-629

SP - 20

EP - 30

JO - Thermochimica Acta

JF - Thermochimica Acta

SN - 0040-6031

ER -