Thermal deformations of the crystal structures of L-valine, L-isoleucine and discrete compound V2I

A.I. Isakov; E.N. Kotelnikova; S.N. Bocharov; Jr. A.A. Zolotarev; H. Lorenz

Thermal deformations of the crystal structures of L-valine, L-isoleucine and discrete compound V2I

A.I. Isakov, E.N. Kotelnikova, S.N. Bocharov, Jr. A.A. Zolotarev, H. Lorenz

Кафедра кристаллографии

Research output

Abstract

Thermal behavior of three phases formed in the system valine—isoleucine was studied by means of temperature-resolved powder diffractometry. Samples were untreated reactants of Val and Ile and precipitate of the discrete compound V2I crystallized from aqueous solu-tion. Investigations were performed from room temperature until substance decomposition temperatures. Thermal deformations of the crystal structures were investigated for all studied phases: parameters of tensor of thermal deformations were calculated and figures of coefficients of thermal expansion of crystal structure were created.

Original language	English
Title of host publication	Proceedings of the 23rd International Workshop on Industrial Crystallization (BIWIC-2013)
Publisher	Cuvillier Verlag
Pages	7-12
Number of pages	6
ISBN (Print)	978-3-7369-9322-8
Publication status	Published - 2016

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title = "Thermal deformations of the crystal structures of L-valine, L-isoleucine and discrete compound V2I",

abstract = "Thermal behavior of three phases formed in the system valine—isoleucine was studied by means of temperature-resolved powder diffractometry. Samples were untreated reactants of Val and Ile and precipitate of the discrete compound V2I crystallized from aqueous solu-tion. Investigations were performed from room temperature until substance decomposition temperatures. Thermal deformations of the crystal structures were investigated for all studied phases: parameters of tensor of thermal deformations were calculated and figures of coefficients of thermal expansion of crystal structure were created.",

keywords = "discrete phases, anomalous racemates, thermal deformations",

author = "A.I. Isakov and E.N. Kotelnikova and S.N. Bocharov and Zolotarev, {Jr. A.A.} and H. Lorenz",

year = "2016",

language = "English",

isbn = "978-3-7369-9322-8",

pages = "7--12",

booktitle = "Proceedings of the 23rd International Workshop on Industrial Crystallization (BIWIC-2013)",

publisher = "Cuvillier Verlag",

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TY - CHAP

T1 - Thermal deformations of the crystal structures of L-valine, L-isoleucine and discrete compound V2I

AU - Isakov, A.I.

AU - Kotelnikova, E.N.

AU - Bocharov, S.N.

AU - Zolotarev, Jr. A.A.

AU - Lorenz, H.

PY - 2016

Y1 - 2016

N2 - Thermal behavior of three phases formed in the system valine—isoleucine was studied by means of temperature-resolved powder diffractometry. Samples were untreated reactants of Val and Ile and precipitate of the discrete compound V2I crystallized from aqueous solu-tion. Investigations were performed from room temperature until substance decomposition temperatures. Thermal deformations of the crystal structures were investigated for all studied phases: parameters of tensor of thermal deformations were calculated and figures of coefficients of thermal expansion of crystal structure were created.

AB - Thermal behavior of three phases formed in the system valine—isoleucine was studied by means of temperature-resolved powder diffractometry. Samples were untreated reactants of Val and Ile and precipitate of the discrete compound V2I crystallized from aqueous solu-tion. Investigations were performed from room temperature until substance decomposition temperatures. Thermal deformations of the crystal structures were investigated for all studied phases: parameters of tensor of thermal deformations were calculated and figures of coefficients of thermal expansion of crystal structure were created.

KW - discrete phases

KW - anomalous racemates

KW - thermal deformations

M3 - Article in an anthology

SN - 978-3-7369-9322-8

SP - 7

EP - 12

BT - Proceedings of the 23rd International Workshop on Industrial Crystallization (BIWIC-2013)

PB - Cuvillier Verlag

ER -