Determination of the phenol index of water by stepwise injection analysis with offline preconcentration by extraction chromatography

A.V. Bulatov, E.A. Mikhailova, I.I. Timofeeva, A.L. Moskvin, L.N. Moskvin

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1 Citation (Scopus)

Abstract

A procedure for the photometry determination of the phenol index of aqueous media is developed, which involves the preliminary separation of alkylphenols and their derivatives from water samples in sampling. Samples are filtered through an extraction chromatography column containing tributyl phosphate as an active component of the stationary phase followed by their quantification under the conditions of stepwise injection analysis. The detection limit of the method is 0.1 μg/L for simple phenol. © 2013 Pleiades Publishing, Ltd.
Original languageEnglish
Pages (from-to)15-18
JournalJournal of Analytical Chemistry
Volume68
Issue number1
DOIs
Publication statusPublished - 2013

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Chromatography
Phenol
Photometry
Column chromatography
Water
Sampling
Derivatives
tributyl phosphate

Cite this

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title = "Determination of the phenol index of water by stepwise injection analysis with offline preconcentration by extraction chromatography",
abstract = "A procedure for the photometry determination of the phenol index of aqueous media is developed, which involves the preliminary separation of alkylphenols and their derivatives from water samples in sampling. Samples are filtered through an extraction chromatography column containing tributyl phosphate as an active component of the stationary phase followed by their quantification under the conditions of stepwise injection analysis. The detection limit of the method is 0.1 μg/L for simple phenol. {\circledC} 2013 Pleiades Publishing, Ltd.",
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AU - Bulatov, A.V.

AU - Mikhailova, E.A.

AU - Timofeeva, I.I.

AU - Moskvin, A.L.

AU - Moskvin, L.N.

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N2 - A procedure for the photometry determination of the phenol index of aqueous media is developed, which involves the preliminary separation of alkylphenols and their derivatives from water samples in sampling. Samples are filtered through an extraction chromatography column containing tributyl phosphate as an active component of the stationary phase followed by their quantification under the conditions of stepwise injection analysis. The detection limit of the method is 0.1 μg/L for simple phenol. © 2013 Pleiades Publishing, Ltd.

AB - A procedure for the photometry determination of the phenol index of aqueous media is developed, which involves the preliminary separation of alkylphenols and their derivatives from water samples in sampling. Samples are filtered through an extraction chromatography column containing tributyl phosphate as an active component of the stationary phase followed by their quantification under the conditions of stepwise injection analysis. The detection limit of the method is 0.1 μg/L for simple phenol. © 2013 Pleiades Publishing, Ltd.

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