Approaches to the Control of Morphological Parameters of Inorganic Nanoparticles in the Synthesis from Solutions

O. M. Osmolovskaya, Yu V. Petukhova, A. A. Podurets, E. A. Syukkalova, V. V. Suslonov, D. S. Kolokolov, S. V. Kotel’nikova, N. P. Bobrysheva, M. G. Osmolowsky

Research outputpeer-review

Abstract

General regularities of nanoparticles formation from solutions under various conditions (organic and aqueous media, mild and rigid conditions) are presented and analyzed. Two ways of a a solid phase formation, based on simultaneous or sequential crystallization, are proposed; examples of the corresponding synthetic procedures are given. The process of sequential crystallization is described. The ability to reduce or increase particle sizes by using morphology control agents has been demonstrated by specific examples. Nucleating agents or nuclei can be successfully used to reduce the size of particles or to obtain the desired crystalline phases (if the compound is characterized by several polymorphs).

Original languageEnglish
Pages (from-to)1154-1161
JournalRussian Journal of General Chemistry
Volume89
Issue number6
DOIs
Publication statusPublished - 1 Jun 2019

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Crystallization
Nanoparticles
Polymorphism
Particle size
Crystalline materials

Scopus subject areas

  • Chemistry(all)

Cite this

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title = "Approaches to the Control of Morphological Parameters of Inorganic Nanoparticles in the Synthesis from Solutions",
abstract = "General regularities of nanoparticles formation from solutions under various conditions (organic and aqueous media, mild and rigid conditions) are presented and analyzed. Two ways of a a solid phase formation, based on simultaneous or sequential crystallization, are proposed; examples of the corresponding synthetic procedures are given. The process of sequential crystallization is described. The ability to reduce or increase particle sizes by using morphology control agents has been demonstrated by specific examples. Nucleating agents or nuclei can be successfully used to reduce the size of particles or to obtain the desired crystalline phases (if the compound is characterized by several polymorphs).",
keywords = "capping agents, hydrothermal synthesis, nanoparticles, polyol synthesis, solvothermal synthesis",
author = "Osmolovskaya, {O. M.} and Petukhova, {Yu V.} and Podurets, {A. A.} and Syukkalova, {E. A.} and Suslonov, {V. V.} and Kolokolov, {D. S.} and Kotel’nikova, {S. V.} and Bobrysheva, {N. P.} and Osmolowsky, {M. G.}",
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language = "English",
volume = "89",
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Approaches to the Control of Morphological Parameters of Inorganic Nanoparticles in the Synthesis from Solutions. / Osmolovskaya, O. M.; Petukhova, Yu V.; Podurets, A. A.; Syukkalova, E. A.; Suslonov, V. V.; Kolokolov, D. S.; Kotel’nikova, S. V.; Bobrysheva, N. P.; Osmolowsky, M. G.

In: Russian Journal of General Chemistry, Vol. 89, No. 6, 01.06.2019, p. 1154-1161.

Research outputpeer-review

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T1 - Approaches to the Control of Morphological Parameters of Inorganic Nanoparticles in the Synthesis from Solutions

AU - Osmolovskaya, O. M.

AU - Petukhova, Yu V.

AU - Podurets, A. A.

AU - Syukkalova, E. A.

AU - Suslonov, V. V.

AU - Kolokolov, D. S.

AU - Kotel’nikova, S. V.

AU - Bobrysheva, N. P.

AU - Osmolowsky, M. G.

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N2 - General regularities of nanoparticles formation from solutions under various conditions (organic and aqueous media, mild and rigid conditions) are presented and analyzed. Two ways of a a solid phase formation, based on simultaneous or sequential crystallization, are proposed; examples of the corresponding synthetic procedures are given. The process of sequential crystallization is described. The ability to reduce or increase particle sizes by using morphology control agents has been demonstrated by specific examples. Nucleating agents or nuclei can be successfully used to reduce the size of particles or to obtain the desired crystalline phases (if the compound is characterized by several polymorphs).

AB - General regularities of nanoparticles formation from solutions under various conditions (organic and aqueous media, mild and rigid conditions) are presented and analyzed. Two ways of a a solid phase formation, based on simultaneous or sequential crystallization, are proposed; examples of the corresponding synthetic procedures are given. The process of sequential crystallization is described. The ability to reduce or increase particle sizes by using morphology control agents has been demonstrated by specific examples. Nucleating agents or nuclei can be successfully used to reduce the size of particles or to obtain the desired crystalline phases (if the compound is characterized by several polymorphs).

KW - capping agents

KW - hydrothermal synthesis

KW - nanoparticles

KW - polyol synthesis

KW - solvothermal synthesis

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